N,N'-bis(2,6-diisopropyl-4-(morpholinomethyl)phenyl)ethylenediimine

Base Information

• Chemical Name: N,N'-bis(2,6-diisopropyl-4-(morpholinomethyl)phenyl)ethylenediimine
• CAS No.: 1129711-19-8
• Molecular Formula: C₃₆H₅₄N₄O₂
• Molecular Weight: 574.85
• Mol file: 1129711-19-8.mol

Synonyms:N,N'-bis(2,6-diisopropyl-4-(morpholinomethyl)phenyl)ethylenediimine

Chemical Property of N,N'-bis(2,6-diisopropyl-4-(morpholinomethyl)phenyl)ethylenediimine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N,N'-bis(2,6-diisopropyl-4-(morpholinomethyl)phenyl)ethylenediimine

There total 2 articles about N,N'-bis(2,6-diisopropyl-4-(morpholinomethyl)phenyl)ethylenediimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

Glyoxal (131543-46-9,107-22-2) + 2,6-diisopropyl-4-(morpholinomethyl)aniline (86519-33-7) → N,N'-bis(2,6-diisopropyl-4-(morpholinomethyl)phenyl)ethylenediimine (1129711-19-8)

Guidance literature:

With formic acid; In methanol; water; at 20 ℃; for 576h;

DOI:10.1039/b820633c

Reference yield:

2,6-diisopropylbenzenamine (24544-04-5) → N,N'-bis(2,6-diisopropyl-4-(morpholinomethyl)phenyl)ethylenediimine (1129711-19-8)

Guidance literature:

Multi-step reaction with 2 steps

1: ethanol; water / Reflux

2: formic acid / methanol / 20 °C

With formic acid; In methanol; ethanol; water;

DOI:10.1039/c3gc36830k

Reference yield: 76.0%

N,N'-bis(2,6-diisopropyl-4-(morpholinomethyl)phenyl)ethylenediimine (1129711-19-8) → N,N'-bis(2,6-diisopropyl-4-(morpholinomethyl)phenyl)ethylenediamine (1129711-25-6)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 - 10 ℃; for 0.5h;

DOI:10.1039/b820633c

upstream raw materials:

Glyoxal

2,6-diisopropyl-4-(morpholinomethyl)aniline

2,6-diisopropylbenzenamine

Downstream raw materials:

N,N'-bis(2,6-diisopropyl-4-(morpholinomethyl)phenyl)ethylenediamine

1,3-bis(2,6-diisopropyl-4-(morpholinomethyl)phenyl)-4,5-dihydro-1H-imidazol-3-ium-chloride

(1,3-bis(2,6-diisopropyl-4-(morpholinomethyl)phenyl)imidazolidin-2-ylidene)copper(I) chloride

(1,3-bis(2,6-diisopropyl-4-(morpholinomethyl)phenyl)imidazolidin-2-ylidene)copper(I) bromide