[[2-Benzyloxycarbonylamino-4-(tert-butyl-dimethyl-silanyloxy)-butyryl]-(4-methoxy-benzyl)-amino]-acetic acid ethyl ester

Base Information

Chemical Name:[[2-Benzyloxycarbonylamino-4-(tert-butyl-dimethyl-silanyloxy)-butyryl]-(4-methoxy-benzyl)-amino]-acetic acid ethyl ester
CAS No.:109164-76-3
Molecular Formula:C₃₀H₄₄N₂O₇Si
Molecular Weight:572.774
Hs Code.:

Synonyms:[[2-Benzyloxycarbonylamino-4-(tert-butyl-dimethyl-silanyloxy)-butyryl]-(4-methoxy-benzyl)-amino]-acetic acid ethyl ester

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Chemical Property of [[2-Benzyloxycarbonylamino-4-(tert-butyl-dimethyl-silanyloxy)-butyryl]-(4-methoxy-benzyl)-amino]-acetic acid ethyl ester

Chemical Property:

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Technology Process of [[2-Benzyloxycarbonylamino-4-(tert-butyl-dimethyl-silanyloxy)-butyryl]-(4-methoxy-benzyl)-amino]-acetic acid ethyl ester

There total 3 articles about [[2-Benzyloxycarbonylamino-4-(tert-butyl-dimethyl-silanyloxy)-butyryl]-(4-methoxy-benzyl)-amino]-acetic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 60857-16-1
N-(4-methoxybenzyl)glycine ethyl ester

: 109392-77-0
2-Benzyloxycarbonylamino-4-(tert-butyl-dimethyl-silanyloxy)-butyric acid

: 109164-76-3
[[2-Benzyloxycarbonylamino-4-(tert-butyl-dimethyl-silanyloxy)-butyryl]-(4-methoxy-benzyl)-amino]-acetic acid ethyl ester

Guidance literature:: With dicyclohexyl-carbodiimide; In tetrahydrofuran; at 25 ℃;
DOI:10.1016/S0040-4039(00)84854-6 DOI:10.1021/jo00227a019

Reference yield:

: 79074-03-6
2-(benzyloxycarbonylamino)-4-hydroxybutanoic acid

: 109164-76-3
[[2-Benzyloxycarbonylamino-4-(tert-butyl-dimethyl-silanyloxy)-butyryl]-(4-methoxy-benzyl)-amino]-acetic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / dimethylformamide / 0 °C

2: DCC / tetrahydrofuran / 25 °C

With triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)84854-6 DOI:10.1021/jo00227a019

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 109164-76-3
[[2-Benzyloxycarbonylamino-4-(tert-butyl-dimethyl-silanyloxy)-butyryl]-(4-methoxy-benzyl)-amino]-acetic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / dimethylformamide / 0 °C

2: DCC / tetrahydrofuran / 25 °C

With triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)84854-6 DOI:10.1021/jo00227a019