Technology Process of C20H33FO4SSi
There total 7 articles about C20H33FO4SSi which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C19H31FO2Si;
With
triethylamine;
In
dichloromethane;
at 0 ℃;
methanesulfonyl chloride;
In
dichloromethane;
at 0 ℃;
for 2.5h;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: sodium methylate / tetrahydrofuran; methanol / 20 - 50 °C
2.1: hydrogenchloride / ethanol; water / 40 h / Reflux
3.1: sodium tetrahydroborate / ethanol / -20 - 20 °C
4.1: 2,6-dimethylpyridine / dichloromethane / 0 - 20 °C
5.1: diisobutylaluminium hydride / dichloromethane / 1.33 h / -70 °C
5.2: 2 h / 20 °C
6.1: sodium tetrahydroborate / methanol / 17 h / 0 - 20 °C
7.1: triethylamine / dichloromethane / 0 °C
7.2: 2.5 h / 0 °C
With
2,6-dimethylpyridine; hydrogenchloride; sodium tetrahydroborate; sodium methylate; diisobutylaluminium hydride; triethylamine;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; water;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 2,6-dimethylpyridine / dichloromethane / 0 - 20 °C
2.1: diisobutylaluminium hydride / dichloromethane / 1.33 h / -70 °C
2.2: 2 h / 20 °C
3.1: sodium tetrahydroborate / methanol / 17 h / 0 - 20 °C
4.1: triethylamine / dichloromethane / 0 °C
4.2: 2.5 h / 0 °C
With
2,6-dimethylpyridine; sodium tetrahydroborate; diisobutylaluminium hydride; triethylamine;
In
methanol; dichloromethane;