5-(4,4-Dimethoxy-butyl)-2,4,4-trimethyl-3-trimethylsilanylmethyl-1-trimethylsilanyloxy-cyclohexene

Base Information

Chemical Name:5-(4,4-Dimethoxy-butyl)-2,4,4-trimethyl-3-trimethylsilanylmethyl-1-trimethylsilanyloxy-cyclohexene
CAS No.:125493-39-2
Molecular Formula:C₂₂H₄₆O₃Si₂
Molecular Weight:414.776
Hs Code.:

Synonyms:5-(4,4-Dimethoxy-butyl)-2,4,4-trimethyl-3-trimethylsilanylmethyl-1-trimethylsilanyloxy-cyclohexene

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Chemical Property of 5-(4,4-Dimethoxy-butyl)-2,4,4-trimethyl-3-trimethylsilanylmethyl-1-trimethylsilanyloxy-cyclohexene

Chemical Property:

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Technology Process of 5-(4,4-Dimethoxy-butyl)-2,4,4-trimethyl-3-trimethylsilanylmethyl-1-trimethylsilanyloxy-cyclohexene

There total 1 articles about 5-(4,4-Dimethoxy-butyl)-2,4,4-trimethyl-3-trimethylsilanylmethyl-1-trimethylsilanyloxy-cyclohexene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75-77-4
chloro-trimethyl-silane

: 13170-43-9
(trimethylsilyl)methylmagnesium chloride

: 125344-26-5
5-(4,4-Dimethoxy-butyl)-2,4,4-trimethyl-cyclohex-2-enone

: 125493-39-2
5-(4,4-Dimethoxy-butyl)-2,4,4-trimethyl-3-trimethylsilanylmethyl-1-trimethylsilanyloxy-cyclohexene

Guidance literature:: copper;
DOI:10.1016/S0040-4039(00)99234-7

Reference yield:

: 125493-39-2
5-(4,4-Dimethoxy-butyl)-2,4,4-trimethyl-3-trimethylsilanylmethyl-1-trimethylsilanyloxy-cyclohexene

: 1193-55-1
2-methylcyclohexane-1,3-dione

: 125344-27-6
5-(4,4-Dimethoxy-butyl)-4,4-dimethyl-2-methylene-3-trimethylsilanylmethyl-cyclohexanone

Guidance literature:: palladium (II) ion;
DOI:10.1016/S0040-4039(00)99234-7

Reference yield:

: 125493-39-2
5-(4,4-Dimethoxy-butyl)-2,4,4-trimethyl-3-trimethylsilanylmethyl-1-trimethylsilanyloxy-cyclohexene

: 125344-34-5
2-Methyl-3-trimethylsilanylmethyl-cyclohex-2-enone

Guidance literature:: Multi-step reaction with 3 steps

1: Pd(II)

2: triphenylphosphine-dibromide, triethylamine

3: 91 percent

With triethylamine; dibromotriphenylphosphorane; palladium (II) ion;
DOI:10.1016/S0040-4039(00)99234-7