4-t-butyl-N-[3-(5,5-dimethyl[1,3,2]dioxaborinan-2-yl)-2-methylphenyl]-benzamide

Base Information

Chemical Name:4-t-butyl-N-[3-(5,5-dimethyl[1,3,2]dioxaborinan-2-yl)-2-methylphenyl]-benzamide
CAS No.:886854-80-4
Molecular Formula:C₂₃H₃₀BNO₃
Molecular Weight:379.307
Hs Code.:

Synonyms:4-t-butyl-N-[3-(5,5-dimethyl[1,3,2]dioxaborinan-2-yl)-2-methylphenyl]-benzamide

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Chemical Property of 4-t-butyl-N-[3-(5,5-dimethyl[1,3,2]dioxaborinan-2-yl)-2-methylphenyl]-benzamide

Chemical Property:

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Technology Process of 4-t-butyl-N-[3-(5,5-dimethyl[1,3,2]dioxaborinan-2-yl)-2-methylphenyl]-benzamide

There total 4 articles about 4-t-butyl-N-[3-(5,5-dimethyl[1,3,2]dioxaborinan-2-yl)-2-methylphenyl]-benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 886854-79-1
3-(5,5-dimethyl[1,3,2]dioxaborinan-2-yl)-2-methylaniline

: 1710-98-1
p-tert-butyl benzoyl chloride

: 886854-80-4
4-t-butyl-N-[3-(5,5-dimethyl[1,3,2]dioxaborinan-2-yl)-2-methylphenyl]-benzamide

Guidance literature:: With triethylamine; In tetrahydrofuran; at 20 ℃; for 0.25h;

Reference yield:

: 886854-78-0
2-(2-methyl-3-nitrophenyl)-5,5-dimethyl[1,3,2]dioxaborinane

: 886854-80-4
4-t-butyl-N-[3-(5,5-dimethyl[1,3,2]dioxaborinan-2-yl)-2-methylphenyl]-benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / palladium 10% on activated carbon / methanol; ethyl acetate / 2 h / 20 °C / 2068.65 Torr

2: triethylamine / tetrahydrofuran / 0.25 h / 20 °C

With hydrogen; triethylamine; palladium 10% on activated carbon; In tetrahydrofuran; methanol; ethyl acetate;

Reference yield:

2-bromo-6-nitrotoluene: 55289-35-5
2-bromo-6-nitrotoluene

: 886854-80-4
4-t-butyl-N-[3-(5,5-dimethyl[1,3,2]dioxaborinan-2-yl)-2-methylphenyl]-benzamide

Guidance literature:: Multi-step reaction with 3 steps

1: potassium acetate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane / 3 h / Heating / reflux

2: hydrogen / palladium 10% on activated carbon / methanol; ethyl acetate / 2 h / 20 °C / 2068.65 Torr

3: triethylamine / tetrahydrofuran / 0.25 h / 20 °C

With hydrogen; potassium acetate; triethylamine; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; palladium 10% on activated carbon; In tetrahydrofuran; 1,4-dioxane; methanol; ethyl acetate;