(2S,4S)-1-((S)-3-Acetylsulfanyl-2-methyl-propionyl)-4-phenoxy-pyrrolidine-2-carboxylic acid

Base Information

Chemical Name:(2S,4S)-1-((S)-3-Acetylsulfanyl-2-methyl-propionyl)-4-phenoxy-pyrrolidine-2-carboxylic acid
CAS No.:113949-46-5
Molecular Formula:C₁₇H₂₁NO₅S
Molecular Weight:351.423
Hs Code.:

Synonyms:(2S,4S)-1-((S)-3-Acetylsulfanyl-2-methyl-propionyl)-4-phenoxy-pyrrolidine-2-carboxylic acid

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Chemical Property of (2S,4S)-1-((S)-3-Acetylsulfanyl-2-methyl-propionyl)-4-phenoxy-pyrrolidine-2-carboxylic acid

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Technology Process of (2S,4S)-1-((S)-3-Acetylsulfanyl-2-methyl-propionyl)-4-phenoxy-pyrrolidine-2-carboxylic acid

There total 3 articles about (2S,4S)-1-((S)-3-Acetylsulfanyl-2-methyl-propionyl)-4-phenoxy-pyrrolidine-2-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 74345-73-6
(2R,S)-3-Acetylthio-2-methylpropanoyl chloride

: 113949-37-4
cis-4-phenoxy-L-propline

: 113949-46-5
(2S,4S)-1-((S)-3-Acetylsulfanyl-2-methyl-propionyl)-4-phenoxy-pyrrolidine-2-carboxylic acid

Guidance literature:: With sodium carbonate; In water; for 1h;
DOI:10.1021/jm00401a014

Reference yield:

: 132592-07-5
(2S,4S)-4-hydroxy-1,2-pyrrolidinedicarboxylic acid 1,2-bis(phenylmethyl ester)

: 113949-46-5
(2S,4S)-1-((S)-3-Acetylsulfanyl-2-methyl-propionyl)-4-phenoxy-pyrrolidine-2-carboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Ph₃P, DEAD, 2.) H₂ / 2.) Pd/C / 1.) THF, room temperature, overnight

2: 25percent sodium carbonate, pH 8.5 / H₂O / 1 h

With hydrogen; sodium carbonate; triphenylphosphine; diethylazodicarboxylate; palladium on activated charcoal; In water;
DOI:10.1021/jm00401a014

Reference yield:

: 108-95-2,27073-41-2
phenol

: 113949-46-5
(2S,4S)-1-((S)-3-Acetylsulfanyl-2-methyl-propionyl)-4-phenoxy-pyrrolidine-2-carboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Ph₃P, DEAD, 2.) H₂ / 2.) Pd/C / 1.) THF, room temperature, overnight

2: 25percent sodium carbonate, pH 8.5 / H₂O / 1 h

With hydrogen; sodium carbonate; triphenylphosphine; diethylazodicarboxylate; palladium on activated charcoal; In water;
DOI:10.1021/jm00401a014