(+/-)-N-acetyl-3-<<(trifluoromethyl)sulfonyl>oxy>phenylalanine phenylmethyl ester

Base Information

Chemical Name:(+/-)-N-acetyl-3-<<(trifluoromethyl)sulfonyl>oxy>phenylalanine phenylmethyl ester
CAS No.:127153-06-4
Molecular Formula:C₁₉H₁₈F₃NO₆S
Molecular Weight:445.416
Hs Code.:

Synonyms:(+/-)-N-acetyl-3-<<(trifluoromethyl)sulfonyl>oxy>phenylalanine phenylmethyl ester

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Chemical Property of (+/-)-N-acetyl-3-<<(trifluoromethyl)sulfonyl>oxy>phenylalanine phenylmethyl ester

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Technology Process of (+/-)-N-acetyl-3-<<(trifluoromethyl)sulfonyl>oxy>phenylalanine phenylmethyl ester

There total 3 articles about (+/-)-N-acetyl-3-<<(trifluoromethyl)sulfonyl>oxy>phenylalanine phenylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 37595-74-7
N,N-phenylbistrifluoromethane-sulfonimide

: 127153-05-3
(+/-)-N-acetyl-3-hydroxyphenylalanine phenylmethyl ester

: 127153-06-4
(+/-)-N-acetyl-3-<<(trifluoromethyl)sulfonyl>oxy>phenylalanine phenylmethyl ester

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 3h;
DOI:10.1021/jm00107a037

Reference yield:

: 775-06-4,29562-33-2
D/L-3-hydroxy-phenylalanine

: 127153-06-4
(+/-)-N-acetyl-3-<<(trifluoromethyl)sulfonyl>oxy>phenylalanine phenylmethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 8.72 g / p-TsOH*H₂O / toluene / 4 h / Heating

2: 84 percent / Na₂CO₃ / CH₂Cl₂ / 1 h

3: 85 percent / Et₃N / CH₂Cl₂ / 3 h / 0 - 20 °C

With sodium carbonate; toluene-4-sulfonic acid; triethylamine; In dichloromethane; toluene;
DOI:10.1021/jm00107a037

Reference yield:

: 127153-04-2
(+/-)-3-hydroxyphenylalanine phenylmethyl ester

: 127153-06-4
(+/-)-N-acetyl-3-<<(trifluoromethyl)sulfonyl>oxy>phenylalanine phenylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / Na₂CO₃ / CH₂Cl₂ / 1 h

2: 85 percent / Et₃N / CH₂Cl₂ / 3 h / 0 - 20 °C

With sodium carbonate; triethylamine; In dichloromethane;
DOI:10.1021/jm00107a037