7-Phenyl-5,6,7,11-tetrahydro-7a,8,10,11-tetraaza-cyclopenta[b]phenanthrene

Base Information

• Chemical Name: 7-Phenyl-5,6,7,11-tetrahydro-7a,8,10,11-tetraaza-cyclopenta[b]phenanthrene
• CAS No.: 134952-52-6
• Molecular Formula: C₁₉H₁₆N₄
• Molecular Weight: 300.363
• Mol file: 134952-52-6.mol

Synonyms:7-Phenyl-5,6,7,11-tetrahydro-7a,8,10,11-tetraaza-cyclopenta[b]phenanthrene

Chemical Property of 7-Phenyl-5,6,7,11-tetrahydro-7a,8,10,11-tetraaza-cyclopenta[b]phenanthrene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 7-Phenyl-5,6,7,11-tetrahydro-7a,8,10,11-tetraaza-cyclopenta[b]phenanthrene

There total 2 articles about 7-Phenyl-5,6,7,11-tetrahydro-7a,8,10,11-tetraaza-cyclopenta[b]phenanthrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

3(5)-amino-1,2,4-triazole (61-82-5) + 2-benzylidene-1-tetralone (6261-32-1) → 7-Phenyl-5,6,7,11-tetrahydro-7a,8,10,11-tetraaza-cyclopenta[b]phenanthrene (134952-52-6)

Guidance literature:

In N,N-dimethyl-formamide; for 1.5h; Heating;

DOI:10.1007/BF00633226

Reference yield: 24.0%

benzaldehyde (100-52-7) + 3-amino-1,2,4-triazole (61-82-5) + 3,4-dihydronaphthalene-1(2H)-one (529-34-0) → 7-Phenyl-5,6,7,11-tetrahydro-7a,8,10,11-tetraaza-cyclopenta[b]phenanthrene (134952-52-6) + 5-Phenyl-4,5,6,7-tetrahydro-1,3,4,11c-tetraaza-cyclopenta[c]phenanthrene + 5-phenyl-6,7-dihydro-1,2,4-triazolo<1,5-a>benzoquinazoline

Guidance literature:

In N,N-dimethyl-formamide; for 3h; Heating;

DOI:10.1007/BF00529878

Reference yield: 73.0%

7-Phenyl-5,6,7,11-tetrahydro-7a,8,10,11-tetraaza-cyclopenta[b]phenanthrene (134952-52-6) → 7-phenyl-5,6-dihydrobenzo[h][1,2,4]triazolo[5,1-b]quinazoline (134952-55-9)

Guidance literature:

With bromine; In acetic acid; Ambient temperature;

DOI:10.1007/BF00633226

upstream raw materials:

3⁽⁵⁾-amino-1,2,4-triazole

2-benzylidene-1-tetralone

benzaldehyde

3-amino-1,2,4-triazole

Downstream raw materials:

7-phenyl-5,6-dihydrobenzo[h][1,2,4]triazolo[5,1-b]quinazoline