((C₆H₅)3P)2N⁽¹⁺⁾*(Ni(CO)3)2P(C₆H₅)2^(1-) = {(Ni(CO)3)2P(C₆H₅)2}{((C₆H₅)3P)2N}

Base Information

Chemical Name:((C₆H₅)3P)2N⁽¹⁺⁾*(Ni(CO)3)2P(C₆H₅)2^(1-) = {(Ni(CO)3)2P(C₆H₅)2}{((C₆H₅)3P)2N}
CAS No.:102982-85-4
Molecular Formula:C₁₈H₁₀Ni₂O₆P*C₃₆H₃₀NP₂
Molecular Weight:1009.22
Hs Code.:

((C<sub>6</sub>H<sub>5</sub>)3P)2N<sup>(1+)</sup>*(Ni(CO)3)2P(C<sub>6</sub>H<sub>5</sub>)2<sup>(1-)</sup> = {(Ni(CO)3)2P(C<sub>6</sub>H<sub>5</sub>)2}{((C<sub>6</sub>H<sub>5</sub>)3P)2N}

Synonyms:((C₆H₅)3P)2N⁽¹⁺⁾*(Ni(CO)3)2P(C₆H₅)2^(1-) = {(Ni(CO)3)2P(C₆H₅)2}{((C₆H₅)3P)2N}

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Chemical Property of ((C₆H₅)3P)2N⁽¹⁺⁾*(Ni(CO)3)2P(C₆H₅)2^(1-) = {(Ni(CO)3)2P(C₆H₅)2}{((C₆H₅)3P)2N}

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Technology Process of ((C₆H₅)3P)2N⁽¹⁺⁾*(Ni(CO)3)2P(C₆H₅)2^(1-) = {(Ni(CO)3)2P(C₆H₅)2}{((C₆H₅)3P)2N}

There total 2 articles about ((C₆H₅)3P)2N⁽¹⁺⁾*(Ni(CO)3)2P(C₆H₅)2^(1-) = {(Ni(CO)3)2P(C₆H₅)2}{((C₆H₅)3P)2N} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 23581-77-3,18399-63-8
{Mo(CO)4(PH(C₆H₅)2)2}

: 917-54-4
methyllithium

: 21050-13-5
bis(triphenylphosphine)iminium chloride

: 13463-39-3,71564-36-8
tetracarbonyl nickel

: 102982-85-4
((C₆H₅)3P)2N⁽¹⁺⁾*(Ni(CO)3)2P(C₆H₅)2^(1-) = {(Ni(CO)3)2P(C₆H₅)2}{((C₆H₅)3P)2N}

: ((C₆H₅)3P)2N⁽¹⁺⁾*((CO)5MoP(C₆H₅)2Ni(CO)3)^(1-) = {(CO)5MoP(C₆H₅)2Ni(CO)3}{((C₆H₅)3P)2N}

Guidance literature:: In diethyl ether; MeLi was added to the Mo-complex in ether; Ni(CO)4 was added; (PNP)Cl (in CH3OH) was added to the lower layer; filtered; dried with N2; recrystd. from CH2Cl2/CH3OH (1:1) containing a small amount Ni(CO)4; elem. anal.;

Reference yield: 69.0%

: 917-54-4
methyllithium

: 21050-13-5
bis(triphenylphosphine)iminium chloride

: 13463-39-3,71564-36-8
tetracarbonyl nickel

: 829-85-6
diphenylphosphane

: 102982-85-4
((C₆H₅)3P)2N⁽¹⁺⁾*(Ni(CO)3)2P(C₆H₅)2^(1-) = {(Ni(CO)3)2P(C₆H₅)2}{((C₆H₅)3P)2N}

Guidance literature:: In methanol; diethyl ether; byproducts: CO; diphenylphosphane was deprotonated with an equimolar amount MeLi; to the solution was added Ni(CO)4; stirred for 2 h; volatiles were removed in vacuo; CH3OH was added; (PNP)Cl was added; filtered; recrystd. from CH3OH/ CH2Cl2; IR;