Technology Process of C43H61NO15
There total 7 articles about C43H61NO15 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogenchloride;
In
methanol; water;
at 35 ℃;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: trifluoroacetic acid / toluene / -15 °C
2.1: dmap; 4-methyl-morpholine; pivaloyl chloride / tetrahydrofuran / 1 h / 38 °C / Inert atmosphere
2.2: 2 °C / pH 1.5 - 1.9
3.1: hydrogenchloride / methanol; water / 35 °C / Inert atmosphere
With
4-methyl-morpholine; hydrogenchloride; dmap; pivaloyl chloride; trifluoroacetic acid;
In
tetrahydrofuran; methanol; water; toluene;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: pyridine / 2 h / -20 - -5.8 °C / Inert atmosphere
2.1: lithium borohydride / tetrahydrofuran; ethanol / -12 - -6.7 °C / Inert atmosphere
3.1: triethylamine; dmap / Isopropyl acetate / 35 °C / Inert atmosphere
4.1: acetic acid / methanol; water / 9 h
5.1: trifluoroacetic acid / toluene / -15 °C
6.1: dmap; 4-methyl-morpholine; pivaloyl chloride / tetrahydrofuran / 1 h / 38 °C / Inert atmosphere
6.2: 2 °C / pH 1.5 - 1.9
7.1: hydrogenchloride / methanol; water / 35 °C / Inert atmosphere
With
4-methyl-morpholine; pyridine; hydrogenchloride; dmap; lithium borohydride; pivaloyl chloride; acetic acid; triethylamine; trifluoroacetic acid;
In
tetrahydrofuran; methanol; ethanol; Isopropyl acetate; water; toluene;