C₁₄H₁₂BrN

Base Information

• Chemical Name: C₁₄H₁₂BrN
• CAS No.: 1433773-40-0
• Molecular Formula: C₁₄H₁₂BrN
• Molecular Weight: 274.16

Synonyms:C₁₄H₁₂BrN

Chemical Property of C₁₄H₁₂BrN

Chemical Property:

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Technology Process of C₁₄H₁₂BrN

There total 4 articles about C₁₄H₁₂BrN which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

N'-(1-(2-aminophenyl)ethylidene)-4-methylbenzenesulfonohydrazide (1433772-22-5) + 2,3-dibromobenzene (583-53-9) → C14H12BrN (1433773-40-0)

Guidance literature:

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; lithium tert-butoxide; ruphos; In 1,4-dioxane; water; at 110 ℃; for 1h; Inert atmosphere; Microwave irradiation;

DOI:10.1002/ejoc.201201070

Reference yield:

(2-bromophenyl)boronic acid (244205-40-1) → C14H12BrN (1433773-40-0)

Guidance literature:

Multi-step reaction with 2 steps

1: palladium(II) trifluoroacetate; methanesulfonic acid; [2,2]bipyridinyl / tetrahydrofuran; water / 36 h / 20 - 80 °C / Schlenk technique

2: potassium tert-butylate / tetrahydrofuran / 5.5 h / 20 - 50 °C / Inert atmosphere

With [2,2]bipyridinyl; methanesulfonic acid; palladium(II) trifluoroacetate; potassium tert-butylate; In tetrahydrofuran; water;

DOI:10.1055/a-1735-6250

Reference yield:

anthranilic acid nitrile (1885-29-6) → C14H12BrN (1433773-40-0)

Guidance literature:

Multi-step reaction with 2 steps

1: palladium(II) trifluoroacetate; methanesulfonic acid; [2,2]bipyridinyl / tetrahydrofuran; water / 36 h / 20 - 80 °C / Schlenk technique

2: potassium tert-butylate / tetrahydrofuran / 5.5 h / 20 - 50 °C / Inert atmosphere

With [2,2]bipyridinyl; methanesulfonic acid; palladium(II) trifluoroacetate; potassium tert-butylate; In tetrahydrofuran; water;

DOI:10.1055/a-1735-6250

upstream raw materials:

N'-(1-(2-aminophenyl)ethylidene)-4-methylbenzenesulfonohydrazide

2,3-dibromobenzene

2-aminoacetophenone

(2-bromophenyl)boronic acid

Downstream raw materials:

9-methyl-acridine

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