2-{n-tetradecyloxy[(4-methoxyphenyl)sulfonyl]amino}acetic acid (tert-butyldimethylsilyl)hydroxyamide

Base Information

Chemical Name:2-{n-tetradecyloxy[(4-methoxyphenyl)sulfonyl]amino}acetic acid (tert-butyldimethylsilyl)hydroxyamide
CAS No.:929224-96-4
Molecular Formula:C₂₉H₅₄N₂O₆SSi
Molecular Weight:586.909
Hs Code.:

Synonyms:2-{n-tetradecyloxy[(4-methoxyphenyl)sulfonyl]amino}acetic acid (tert-butyldimethylsilyl)hydroxyamide

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Chemical Property of 2-{n-tetradecyloxy[(4-methoxyphenyl)sulfonyl]amino}acetic acid (tert-butyldimethylsilyl)hydroxyamide

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Technology Process of 2-{n-tetradecyloxy[(4-methoxyphenyl)sulfonyl]amino}acetic acid (tert-butyldimethylsilyl)hydroxyamide

There total 5 articles about 2-{n-tetradecyloxy[(4-methoxyphenyl)sulfonyl]amino}acetic acid (tert-butyldimethylsilyl)hydroxyamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 4.0%

: 929224-90-8
{n-tetradecyloxy[(4-methoxyphenyl)sulfonyl]amino}acetic acid

: 41879-39-4
O-(tert-butyldimethylsilanyl)hydroxylamine

: 929224-96-4
2-{n-tetradecyloxy[(4-methoxyphenyl)sulfonyl]amino}acetic acid (tert-butyldimethylsilyl)hydroxyamide

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 20h;
DOI:10.1016/j.bmc.2007.01.023

Reference yield:

: 929224-81-7
N-n-tetradecyloxy-4-methoxybenzenesulfonamide

: 929224-96-4
2-{n-tetradecyloxy[(4-methoxyphenyl)sulfonyl]amino}acetic acid (tert-butyldimethylsilyl)hydroxyamide

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / cesium carbonate; tetrabutylammonium hydrogensulfate / dimethylformamide / 72 h / 20 °C

2: 92 percent / trifluoroacetic acid / CH₂Cl₂ / 5 h / 0 °C

3: 4 percent / 1-[3-(dimethylamino)propyl]-3-ethylcarbodiimide HCl / CH₂Cl₂ / 20 h / 20 °C

With tetra(n-butyl)ammonium hydrogensulfate; caesium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2007.01.023

Reference yield:

: 929224-85-1
tert-butyl {n-tetradecyloxy[(4-methoxyphenyl)sulfonyl]amino}acetate

: 929224-96-4
2-{n-tetradecyloxy[(4-methoxyphenyl)sulfonyl]amino}acetic acid (tert-butyldimethylsilyl)hydroxyamide

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / trifluoroacetic acid / CH₂Cl₂ / 5 h / 0 °C

2: 4 percent / 1-[3-(dimethylamino)propyl]-3-ethylcarbodiimide HCl / CH₂Cl₂ / 20 h / 20 °C

With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; In dichloromethane;
DOI:10.1016/j.bmc.2007.01.023