2-carboxy-2-deoxy-3,6-di-O-benzyl-4-(2,3,4,6-tetra-O-benzyl-β-galactopyranosyl)-α-D-glucopyranosyl n-butyl β-aminolactam

Base Information

Chemical Name:2-carboxy-2-deoxy-3,6-di-O-benzyl-4-(2,3,4,6-tetra-O-benzyl-β-galactopyranosyl)-α-D-glucopyranosyl n-butyl β-aminolactam
CAS No.:850908-02-0
Molecular Formula:C₅₉H₆₅NO₁₀
Molecular Weight:948.166
Hs Code.:

Synonyms:2-carboxy-2-deoxy-3,6-di-O-benzyl-4-(2,3,4,6-tetra-O-benzyl-β-galactopyranosyl)-α-D-glucopyranosyl n-butyl β-aminolactam

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Chemical Property of 2-carboxy-2-deoxy-3,6-di-O-benzyl-4-(2,3,4,6-tetra-O-benzyl-β-galactopyranosyl)-α-D-glucopyranosyl n-butyl β-aminolactam

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Technology Process of 2-carboxy-2-deoxy-3,6-di-O-benzyl-4-(2,3,4,6-tetra-O-benzyl-β-galactopyranosyl)-α-D-glucopyranosyl n-butyl β-aminolactam

There total 4 articles about 2-carboxy-2-deoxy-3,6-di-O-benzyl-4-(2,3,4,6-tetra-O-benzyl-β-galactopyranosyl)-α-D-glucopyranosyl n-butyl β-aminolactam which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 850908-01-9
2-carboxy-2-deoxy-3,6-di-O-benzyl-4-(2,3,4,6-tetra-O-benzyl-β-galactopyranosyl)-α-D-glucopyranosyl β-aminolactam

: 109-65-9
1-bromo-butane

: 850908-02-0
2-carboxy-2-deoxy-3,6-di-O-benzyl-4-(2,3,4,6-tetra-O-benzyl-β-galactopyranosyl)-α-D-glucopyranosyl n-butyl β-aminolactam

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 3h;
DOI:10.1039/b418247b

Reference yield:

: 1054681-39-8
(1S,3R,4S,5R,6R)-5-Benzyloxy-3-benzyloxymethyl-8-(2,2,2-trichloro-acetyl)-4-((2S,3R,4S,5S,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yloxy)-2-oxa-8-aza-bicyclo[4.2.0]octan-7-one

: 850908-02-0
2-carboxy-2-deoxy-3,6-di-O-benzyl-4-(2,3,4,6-tetra-O-benzyl-β-galactopyranosyl)-α-D-glucopyranosyl n-butyl β-aminolactam

Guidance literature:: Multi-step reaction with 2 steps

1: 275 mg / benzylamine / -20 °C

2: 80 percent / NaH / dimethylformamide / 3 h / 0 °C

With sodium hydride; benzylamine; In N,N-dimethyl-formamide;
DOI:10.1039/b418247b

Reference yield:

: 114117-12-3
2,3,4,6-tetra-O-benzyl-β-D-galactopyranosyl-(1->4)-1,5-anhydro-2-deoxy-3,6-di-O-benzyl-D-arabino-hex-1-enitol

: 850908-02-0
2-carboxy-2-deoxy-3,6-di-O-benzyl-4-(2,3,4,6-tetra-O-benzyl-β-galactopyranosyl)-α-D-glucopyranosyl n-butyl β-aminolactam

Guidance literature:: Multi-step reaction with 3 steps

1: CHCl₃ / 18 h / 20 °C

2: 275 mg / benzylamine / -20 °C

3: 80 percent / NaH / dimethylformamide / 3 h / 0 °C

With sodium hydride; benzylamine; In chloroform; N,N-dimethyl-formamide;
DOI:10.1039/b418247b