C₁₅H₂₀O₅

Base Information

Chemical Name:C₁₅H₂₀O₅
CAS No.:1612882-46-8
Molecular Formula:C₁₅H₂₀O₅
Molecular Weight:280.321
Hs Code.:

C<sub>15</sub>H<sub>20</sub>O<sub>5</sub>

Synonyms:C₁₅H₂₀O₅

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₅H₂₀O₅

Chemical Property:

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Technology Process of C₁₅H₂₀O₅

There total 6 articles about C₁₅H₂₀O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1612882-37-7
C₁₀H₁₃IO

: 108-59-8
malonic acid dimethyl ester

: 1612882-46-8
C₁₅H₂₀O₅

Guidance literature:: malonic acid dimethyl ester; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 ℃; for 0.25h;

C₁₀H₁₃IO; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 13h;
DOI:10.1002/adsc.201300250

Reference yield:

: 3698-28-0
2-allylanisole

: 1612882-46-8
C₁₅H₂₀O₅

Guidance literature:: Multi-step reaction with 6 steps

1.1: ozone / dichloromethane / 0.17 h / -78 °C

1.2: 12 h / 20 °C

2.1: (5S)-(?)-2,2,3-trimethyl-5-benzyl-4-imidazolidinone monohydrochloride / water; acetonitrile / 24 h / 0 °C

3.1: sodium tetrahydroborate / methanol / 0.5 h / 0 °C

4.1: hydrogen / water; ethanol / 3 h / 760.05 Torr

5.1: iodine; 1H-imidazole; triphenylphosphine / acetonitrile; diethyl ether / 4.5 h / 20 °C

6.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.25 h / 0 °C

6.2: 13 h / 20 °C

With 1H-imidazole; sodium tetrahydroborate; hydrogen; iodine; sodium hydride; ozone; triphenylphosphine; (5S)-(?)-2,2,3-trimethyl-5-benzyl-4-imidazolidinone monohydrochloride; In methanol; diethyl ether; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; mineral oil;
DOI:10.1002/adsc.201300250

Reference yield:

: 1612882-09-3
C₁₆H₁₄O₂S₂

: 1612882-46-8
C₁₅H₂₀O₅

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium tetrahydroborate / methanol / 0.5 h / 0 °C

2.1: hydrogen / water; ethanol / 3 h / 760.05 Torr

3.1: iodine; 1H-imidazole; triphenylphosphine / acetonitrile; diethyl ether / 4.5 h / 20 °C

4.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.25 h / 0 °C

4.2: 13 h / 20 °C

With 1H-imidazole; sodium tetrahydroborate; hydrogen; iodine; sodium hydride; triphenylphosphine; In methanol; diethyl ether; ethanol; water; N,N-dimethyl-formamide; acetonitrile; mineral oil;
DOI:10.1002/adsc.201300250