methyl 2-(tert-butoxycarbonylamino)-4-(((3aS,4S,6R,6aR)-2,2-dimethyl-6-(6-(phenethylamino)-9H-purin-9-yl)-tetrahydrofuro[3,4-d][1,3]dioxol-4-yl)methylthio)butanoate

Base Information

Chemical Name:methyl 2-(tert-butoxycarbonylamino)-4-(((3aS,4S,6R,6aR)-2,2-dimethyl-6-(6-(phenethylamino)-9H-purin-9-yl)-tetrahydrofuro[3,4-d][1,3]dioxol-4-yl)methylthio)butanoate
CAS No.:901776-24-7
Molecular Formula:C₃₁H₄₂N₆O₇S
Molecular Weight:642.776
Hs Code.:

methyl 2-(tert-butoxycarbonylamino)-4-(((3aS,4S,6R,6aR)-2,2-dimethyl-6-(6-(phenethylamino)-9H-purin-9-yl)-tetrahydrofuro[3,4-d][1,3]dioxol-4-yl)methylthio)butanoate

Synonyms:methyl 2-(tert-butoxycarbonylamino)-4-(((3aS,4S,6R,6aR)-2,2-dimethyl-6-(6-(phenethylamino)-9H-purin-9-yl)-tetrahydrofuro[3,4-d][1,3]dioxol-4-yl)methylthio)butanoate

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Chemical Property of methyl 2-(tert-butoxycarbonylamino)-4-(((3aS,4S,6R,6aR)-2,2-dimethyl-6-(6-(phenethylamino)-9H-purin-9-yl)-tetrahydrofuro[3,4-d][1,3]dioxol-4-yl)methylthio)butanoate

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Technology Process of methyl 2-(tert-butoxycarbonylamino)-4-(((3aS,4S,6R,6aR)-2,2-dimethyl-6-(6-(phenethylamino)-9H-purin-9-yl)-tetrahydrofuro[3,4-d][1,3]dioxol-4-yl)methylthio)butanoate

There total 1 articles about methyl 2-(tert-butoxycarbonylamino)-4-(((3aS,4S,6R,6aR)-2,2-dimethyl-6-(6-(phenethylamino)-9H-purin-9-yl)-tetrahydrofuro[3,4-d][1,3]dioxol-4-yl)methylthio)butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 901776-23-6
((3aR,4R,6R,6aR)-2,2-dimethyl-6-(6-(phenethylamino)-9H-purin-9-yl)-tetrahydrofuro[3,4-d][1,3]dioxol-4-yl)methanol

: 124-41-4
sodium methylate

: 130288-32-3
tert-butyl (2-oxotetrahydrothiophen-3-yl)carbamate

: 901776-24-7
methyl 2-(tert-butoxycarbonylamino)-4-(((3aS,4S,6R,6aR)-2,2-dimethyl-6-(6-(phenethylamino)-9H-purin-9-yl)-tetrahydrofuro[3,4-d][1,3]dioxol-4-yl)methylthio)butanoate

Guidance literature:: ((3aR,4R,6R,6aR)-2,2-dimethyl-6-(6-(phenethylamino)-9H-purin-9-yl)-tetrahydrofuro[3,4-d][1,3]dioxol-4-yl)methanol; With sodium hydride; In tetrahydrofuran; at 0 ℃; for 0.25h;

With p-toluenesulfonyl chloride; In tetrahydrofuran; at 0 ℃; for 1h;

sodium methylate; tert-butyl (2-oxotetrahydrothiophen-3-yl)carbamate; In methanol; at 20 ℃; for 4.25h; Heating / reflux;

Reference yield: 40.0%

: 901776-24-7
methyl 2-(tert-butoxycarbonylamino)-4-(((3aS,4S,6R,6aR)-2,2-dimethyl-6-(6-(phenethylamino)-9H-purin-9-yl)-tetrahydrofuro[3,4-d][1,3]dioxol-4-yl)methylthio)butanoate

: 901775-20-0
2-amino-4-(((2S,3S,4R,5R)-3,4-dihydroxy-5-(6-(phenethylamino)-9H-purin-9-yl)-tetrahydrofuran-2-yl)methylthio)butanoic acid

Guidance literature:: methyl 2-(tert-butoxycarbonylamino)-4-(((3aS,4S,6R,6aR)-2,2-dimethyl-6-(6-(phenethylamino)-9H-purin-9-yl)-tetrahydrofuro[3,4-d][1,3]dioxol-4-yl)methylthio)butanoate; With potassium hydroxide; water; In tetrahydrofuran; at 20 ℃; for 2h;

With citric acid; In water; pH=2;

With 2,6-di-tert-butyl-4-methyl-phenol; ammonia; water; trifluoroacetic acid; more than 3 stages;