Technology Process of 5-(tert-butyldiphenylsiloxy)hexanal
There total 6 articles about 5-(tert-butyldiphenylsiloxy)hexanal which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
pyridinium chlorochromate;
In
dichloromethane;
at 20 ℃;
for 1h;
DOI:10.1055/s-0031-1289643
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: pyridinium chlorochromate / dichloromethane / 1 h / 20 °C
2.1: magnesium / diethyl ether / Reflux
2.2: 2 h / 0 - 20 °C
3.1: 1H-imidazole; dmap / dichloromethane / 2 h / 0 - 20 °C
4.1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 10 h / 2850.29 Torr
5.1: pyridinium chlorochromate / dichloromethane / 1 h / 20 °C
With
1H-imidazole; dmap; palladium 10% on activated carbon; hydrogen; magnesium; pyridinium chlorochromate;
In
diethyl ether; dichloromethane; ethyl acetate;
DOI:10.1055/s-0031-1289643
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1H-imidazole; dmap / dichloromethane / 2 h / 0 - 20 °C
2: palladium 10% on activated carbon; hydrogen / ethyl acetate / 10 h / 2850.29 Torr
3: pyridinium chlorochromate / dichloromethane / 1 h / 20 °C
With
1H-imidazole; dmap; palladium 10% on activated carbon; hydrogen; pyridinium chlorochromate;
In
dichloromethane; ethyl acetate;
DOI:10.1055/s-0031-1289643
