(1-phenylvinyl)((trimethylsilyl)chloromethyl)dimethylsilane

Base Information

• Chemical Name: (1-phenylvinyl)((trimethylsilyl)chloromethyl)dimethylsilane
• CAS No.: 96430-48-7
• Molecular Formula: C₁₄H₂₃ClSi₂
• Molecular Weight: 282.961
• Mol file: 96430-48-7.mol

Synonyms:(1-phenylvinyl)((trimethylsilyl)chloromethyl)dimethylsilane

Chemical Property of (1-phenylvinyl)((trimethylsilyl)chloromethyl)dimethylsilane

Chemical Property:

Purity/Quality:

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Technology Process of (1-phenylvinyl)((trimethylsilyl)chloromethyl)dimethylsilane

There total 1 articles about (1-phenylvinyl)((trimethylsilyl)chloromethyl)dimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

((trimethylsilyl)chloromethyl)dimethylchlorosilane (18140-01-7) + 1-bromovinylbenzene (98-81-7) → (1-phenylvinyl)((trimethylsilyl)chloromethyl)dimethylsilane (96430-48-7)

Guidance literature:

With tert.-butyl lithium; In diethyl ether; 1.) 1 h; 2.) -23 deg C to RT;

DOI:10.1021/ja00299a031

Reference yield:

(1-phenylvinyl)((trimethylsilyl)chloromethyl)dimethylsilane (96430-48-7) → chloro-trimethyl-silane (75-77-4) + (1-phenyl-2-(trimethylsilyl)cyclopropyl)dimethylchlorosilane (96430-49-8)

Guidance literature:

With aluminium trichloride; In carbon disulfide; at 46 ℃; for 10h;

DOI:10.1021/ja00299a031

upstream raw materials:

((trimethylsilyl)chloromethyl)dimethylchlorosilane

1-bromovinylbenzene

Downstream raw materials:

chloro-trimethyl-silane

(1-phenyl-2-(trimethylsilyl)cyclopropyl)dimethylchlorosilane