9-(2-Bromo-benzyl)-1-(2-bromo-benzyloxy)-9-aza-tricyclo[6.2.2.0^2,7]dodeca-2,4,6,11-tetraen-10-one

Base Information

• Chemical Name: 9-(2-Bromo-benzyl)-1-(2-bromo-benzyloxy)-9-aza-tricyclo[6.2.2.0^2,7]dodeca-2,4,6,11-tetraen-10-one
• CAS No.: 123100-44-7
• Molecular Formula: C₂₅H₁₉Br₂NO₂
• Molecular Weight: 525.239

Synonyms:9-(2-Bromo-benzyl)-1-(2-bromo-benzyloxy)-9-aza-tricyclo[6.2.2.0^2,7]dodeca-2,4,6,11-tetraen-10-one

Chemical Property of 9-(2-Bromo-benzyl)-1-(2-bromo-benzyloxy)-9-aza-tricyclo[6.2.2.0^2,7]dodeca-2,4,6,11-tetraen-10-one

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Technology Process of 9-(2-Bromo-benzyl)-1-(2-bromo-benzyloxy)-9-aza-tricyclo[6.2.2.0^2,7]dodeca-2,4,6,11-tetraen-10-one

There total 3 articles about 9-(2-Bromo-benzyl)-1-(2-bromo-benzyloxy)-9-aza-tricyclo[6.2.2.0^2,7]dodeca-2,4,6,11-tetraen-10-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

2-carboxybenzene diazonium chloride (4661-46-5) + N-(2-bromobenzyl)-3-<(2-bromobenzyl)oxy>-2(1H)-pyridone (123100-43-6) → 9-(2-Bromo-benzyl)-1-(2-bromo-benzyloxy)-9-aza-tricyclo[6.2.2.02,7]dodeca-2,4,6,11-tetraen-10-one (123100-44-7)

Guidance literature:

With methyloxirane; In 1,2-dichloro-ethane; for 15h; Heating;

DOI:10.1021/jo00282a022

Reference yield:

dihydroxypyridine (16867-04-2) → 9-(2-Bromo-benzyl)-1-(2-bromo-benzyloxy)-9-aza-tricyclo[6.2.2.02,7]dodeca-2,4,6,11-tetraen-10-one (123100-44-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) potassium carbonate / 1.) DME, reflux, 1 h, 2.) reflux, 16 h

2: 75 percent / propylene oxide / 1,2-dichloro-ethane / 15 h / Heating

With potassium carbonate; methyloxirane; In 1,2-dichloro-ethane;

DOI:10.1021/jo00282a022

Reference yield:

1-Bromo-2-bromomethyl-benzene (3433-80-5) → 9-(2-Bromo-benzyl)-1-(2-bromo-benzyloxy)-9-aza-tricyclo[6.2.2.02,7]dodeca-2,4,6,11-tetraen-10-one (123100-44-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) potassium carbonate / 1.) DME, reflux, 1 h, 2.) reflux, 16 h

2: 75 percent / propylene oxide / 1,2-dichloro-ethane / 15 h / Heating

With potassium carbonate; methyloxirane; In 1,2-dichloro-ethane;

DOI:10.1021/jo00282a022

upstream raw materials:

2-carboxybenzene diazonium chloride

N-(2-bromobenzyl)-3-<(2-bromobenzyl)oxy>-2(1H)-pyridone

dihydroxypyridine

1-Bromo-2-bromomethyl-benzene

Downstream raw materials:

C₂₅H₂₁NO₂

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