N-methanesulfonyl-1-(3,4-dimethoxy)benzyl-1,2,3,4-tetrahydro-6-benzyloxy-7-methoxyisoquinoline

Base Information

Chemical Name:N-methanesulfonyl-1-(3,4-dimethoxy)benzyl-1,2,3,4-tetrahydro-6-benzyloxy-7-methoxyisoquinoline
CAS No.:329772-74-9
Molecular Formula:C₂₇H₃₁NO₆S
Molecular Weight:497.612
Hs Code.:

Synonyms:N-methanesulfonyl-1-(3,4-dimethoxy)benzyl-1,2,3,4-tetrahydro-6-benzyloxy-7-methoxyisoquinoline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-methanesulfonyl-1-(3,4-dimethoxy)benzyl-1,2,3,4-tetrahydro-6-benzyloxy-7-methoxyisoquinoline

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Technology Process of N-methanesulfonyl-1-(3,4-dimethoxy)benzyl-1,2,3,4-tetrahydro-6-benzyloxy-7-methoxyisoquinoline

There total 1 articles about N-methanesulfonyl-1-(3,4-dimethoxy)benzyl-1,2,3,4-tetrahydro-6-benzyloxy-7-methoxyisoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 54881-16-2
1-(3,4-dimethoxy)benzyl-1,2,3,4-tetrahydro-6-benzyloxy-7-methoxyisoquinoline

: 124-63-0
methanesulfonyl chloride

: 329772-74-9
N-methanesulfonyl-1-(3,4-dimethoxy)benzyl-1,2,3,4-tetrahydro-6-benzyloxy-7-methoxyisoquinoline

Guidance literature:: With potassium carbonate; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1016/S0040-4020(00)00934-0

Reference yield: 84.0%

: 329772-74-9
N-methanesulfonyl-1-(3,4-dimethoxy)benzyl-1,2,3,4-tetrahydro-6-benzyloxy-7-methoxyisoquinoline

: 329772-79-4
N-methanesulfonyl-1-(3,4-dimethoxy)benzyl-1,2,3,4-tetrahydro-7-methoxyisoquinolin-6-ol

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; at 20 ℃; for 2h; under 760 Torr;
DOI:10.1016/S0040-4020(00)00934-0

Reference yield:

: 329772-74-9
N-methanesulfonyl-1-(3,4-dimethoxy)benzyl-1,2,3,4-tetrahydro-6-benzyloxy-7-methoxyisoquinoline

: 329772-84-1
N-methanesulfonyl-1-(3,4-dimethoxy)benzyl-7-acetoxy-1,2,3,4,6,7-hexahydro-7-methoxy-6-oxoisoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / H₂ / Pd/C / ethyl acetate / 2 h / 20 °C / 760 Torr

2: CH₂Cl₂ / 0.5 h

With hydrogen; palladium on activated charcoal; In dichloromethane; ethyl acetate;
DOI:10.1016/S0040-4020(00)00934-0