N-cyclopropyl-N-(2,3-dichlorobenzyl)-2-{4-[2-(2,6-dichloro-4-methylphenoxy)ethoxy]benzyl}pent-4-enamide

Base Information

Chemical Name:N-cyclopropyl-N-(2,3-dichlorobenzyl)-2-{4-[2-(2,6-dichloro-4-methylphenoxy)ethoxy]benzyl}pent-4-enamide
CAS No.:1056554-96-1
Molecular Formula:C₃₁H₃₁Cl₄NO₃
Molecular Weight:607.404
Hs Code.:

Synonyms:N-cyclopropyl-N-(2,3-dichlorobenzyl)-2-{4-[2-(2,6-dichloro-4-methylphenoxy)ethoxy]benzyl}pent-4-enamide

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Chemical Property of N-cyclopropyl-N-(2,3-dichlorobenzyl)-2-{4-[2-(2,6-dichloro-4-methylphenoxy)ethoxy]benzyl}pent-4-enamide

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Technology Process of N-cyclopropyl-N-(2,3-dichlorobenzyl)-2-{4-[2-(2,6-dichloro-4-methylphenoxy)ethoxy]benzyl}pent-4-enamide

There total 7 articles about N-cyclopropyl-N-(2,3-dichlorobenzyl)-2-{4-[2-(2,6-dichloro-4-methylphenoxy)ethoxy]benzyl}pent-4-enamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 625437-42-5
cyclopropyl-(2,3-dichlorobenzyl)amine

: 1056554-95-0
2-{4-[(2,6-dichloro-4-methylphenoxy)ethoxy]benzyl}pent-4-enoic acid

: 1056554-96-1
N-cyclopropyl-N-(2,3-dichlorobenzyl)-2-{4-[2-(2,6-dichloro-4-methylphenoxy)ethoxy]benzyl}pent-4-enamide

Guidance literature:: With N-ethyl-N,N-diisopropylamine; HATU; In N,N-dimethyl-formamide; at 20 ℃; for 12h;

Reference yield:

: 1056555-58-8
ethyl 2-[4-(2-hydroxyethoxy)benzyl]pent-4-enoate

: 1056554-96-1
N-cyclopropyl-N-(2,3-dichlorobenzyl)-2-{4-[2-(2,6-dichloro-4-methylphenoxy)ethoxy]benzyl}pent-4-enamide

Guidance literature:: Multi-step reaction with 3 steps

1: tributylphosphine; 1,1'-azodicarbonyl-dipiperidine / toluene / 2 h / 80 °C

2: methanol; lithium hydroxide; water / tetrahydrofuran / 12 h / 50 °C

3: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 12 h / 20 °C

With methanol; lithium hydroxide; tributylphosphine; water; N-ethyl-N,N-diisopropylamine; HATU; 1,1'-azodicarbonyl-dipiperidine; In tetrahydrofuran; N,N-dimethyl-formamide; toluene;

Reference yield:

: 1056555-57-7
ethyl 2-[4-(2-{[tert-butyl(dimethyl)silyl]oxy}ethoxy)benzyl]pent-4-enoate

: 1056554-96-1
N-cyclopropyl-N-(2,3-dichlorobenzyl)-2-{4-[2-(2,6-dichloro-4-methylphenoxy)ethoxy]benzyl}pent-4-enamide

Guidance literature:: Multi-step reaction with 4 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C

2: tributylphosphine; 1,1'-azodicarbonyl-dipiperidine / toluene / 2 h / 80 °C

3: methanol; lithium hydroxide; water / tetrahydrofuran / 12 h / 50 °C

4: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 12 h / 20 °C

With methanol; lithium hydroxide; tributylphosphine; tetrabutyl ammonium fluoride; water; N-ethyl-N,N-diisopropylamine; HATU; 1,1'-azodicarbonyl-dipiperidine; In tetrahydrofuran; N,N-dimethyl-formamide; toluene;