N-cyclopropyl-N-(2,3-dichlorobenzyl)-2-{4-[2-(2,6-dichloro-4-methylphenoxy)ethoxy]benzyl}-4-hydroxybutanamide

Base Information

Chemical Name:N-cyclopropyl-N-(2,3-dichlorobenzyl)-2-{4-[2-(2,6-dichloro-4-methylphenoxy)ethoxy]benzyl}-4-hydroxybutanamide
CAS No.:1056554-97-2
Molecular Formula:C₃₀H₃₁Cl₄NO₄
Molecular Weight:611.392
Hs Code.:

Synonyms:N-cyclopropyl-N-(2,3-dichlorobenzyl)-2-{4-[2-(2,6-dichloro-4-methylphenoxy)ethoxy]benzyl}-4-hydroxybutanamide

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Chemical Property of N-cyclopropyl-N-(2,3-dichlorobenzyl)-2-{4-[2-(2,6-dichloro-4-methylphenoxy)ethoxy]benzyl}-4-hydroxybutanamide

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Technology Process of N-cyclopropyl-N-(2,3-dichlorobenzyl)-2-{4-[2-(2,6-dichloro-4-methylphenoxy)ethoxy]benzyl}-4-hydroxybutanamide

There total 7 articles about N-cyclopropyl-N-(2,3-dichlorobenzyl)-2-{4-[2-(2,6-dichloro-4-methylphenoxy)ethoxy]benzyl}-4-hydroxybutanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1056554-96-1
N-cyclopropyl-N-(2,3-dichlorobenzyl)-2-{4-[2-(2,6-dichloro-4-methylphenoxy)ethoxy]benzyl}pent-4-enamide

: 1056554-97-2
N-cyclopropyl-N-(2,3-dichlorobenzyl)-2-{4-[2-(2,6-dichloro-4-methylphenoxy)ethoxy]benzyl}-4-hydroxybutanamide

Guidance literature:: N-cyclopropyl-N-(2,3-dichlorobenzyl)-2-{4-[2-(2,6-dichloro-4-methylphenoxy)ethoxy]benzyl}pent-4-enamide; With ozone; In tetrahydrofuran; methanol; at -78 ℃; for 0.333333h;

With sodium tetrahydroborate; In tetrahydrofuran; methanol; at -78 - 20 ℃; for 16h;

With sodium hydroxide; water;

Reference yield:

: 1056555-58-8
ethyl 2-[4-(2-hydroxyethoxy)benzyl]pent-4-enoate

: 1056554-97-2
N-cyclopropyl-N-(2,3-dichlorobenzyl)-2-{4-[2-(2,6-dichloro-4-methylphenoxy)ethoxy]benzyl}-4-hydroxybutanamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: tributylphosphine; 1,1'-azodicarbonyl-dipiperidine / toluene / 2 h / 80 °C

2.1: methanol; lithium hydroxide; water / tetrahydrofuran / 12 h / 50 °C

3.1: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 12 h / 20 °C

4.1: ozone / tetrahydrofuran; methanol / 0.33 h / -78 °C

4.2: 16 h / -78 - 20 °C

With methanol; lithium hydroxide; tributylphosphine; water; ozone; N-ethyl-N,N-diisopropylamine; HATU; 1,1'-azodicarbonyl-dipiperidine; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; toluene;

Reference yield:

: 1056555-57-7
ethyl 2-[4-(2-{[tert-butyl(dimethyl)silyl]oxy}ethoxy)benzyl]pent-4-enoate

: 1056554-97-2
N-cyclopropyl-N-(2,3-dichlorobenzyl)-2-{4-[2-(2,6-dichloro-4-methylphenoxy)ethoxy]benzyl}-4-hydroxybutanamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C

2.1: tributylphosphine; 1,1'-azodicarbonyl-dipiperidine / toluene / 2 h / 80 °C

3.1: methanol; lithium hydroxide; water / tetrahydrofuran / 12 h / 50 °C

4.1: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 12 h / 20 °C

5.1: ozone / tetrahydrofuran; methanol / 0.33 h / -78 °C

5.2: 16 h / -78 - 20 °C

With methanol; lithium hydroxide; tributylphosphine; tetrabutyl ammonium fluoride; water; ozone; N-ethyl-N,N-diisopropylamine; HATU; 1,1'-azodicarbonyl-dipiperidine; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; toluene;