4-(2-{benzyl-[2-(4-benzyloxyphenyl)-ethyl]-amino}-propionyl)phenyl methanesulfonate

Base Information

Chemical Name:4-(2-{benzyl-[2-(4-benzyloxyphenyl)-ethyl]-amino}-propionyl)phenyl methanesulfonate
CAS No.:1345518-18-4
Molecular Formula:C₃₂H₃₃NO₅S
Molecular Weight:543.684
Hs Code.:

Synonyms:4-(2-{benzyl-[2-(4-benzyloxyphenyl)-ethyl]-amino}-propionyl)phenyl methanesulfonate

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Chemical Property of 4-(2-{benzyl-[2-(4-benzyloxyphenyl)-ethyl]-amino}-propionyl)phenyl methanesulfonate

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Technology Process of 4-(2-{benzyl-[2-(4-benzyloxyphenyl)-ethyl]-amino}-propionyl)phenyl methanesulfonate

There total 2 articles about 4-(2-{benzyl-[2-(4-benzyloxyphenyl)-ethyl]-amino}-propionyl)phenyl methanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 635304-58-4
1-[4-(methanesulfonyloxy)phenyl]-2-bromo-1-propanone

: 32293-42-8
benzyl-[2-(4-benzyloxyphenyl)-ethyl]-amine

: 1345518-18-4
4-(2-{benzyl-[2-(4-benzyloxyphenyl)-ethyl]-amino}-propionyl)phenyl methanesulfonate

Guidance literature:: With triethylamine; In ethanol; for 18h; Product distribution / selectivity; Reflux;

Reference yield:

: 929431-57-2
p-(methanesulfonyloxy)propiophenone

: 1345518-18-4
4-(2-{benzyl-[2-(4-benzyloxyphenyl)-ethyl]-amino}-propionyl)phenyl methanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: bromine; hydrogen bromide; acetic acid / dichloromethane / 1 h / 0 °C

2: triethylamine / ethanol / 18 h / Reflux

With hydrogen bromide; bromine; acetic acid; triethylamine; In ethanol; dichloromethane;

Reference yield: 96.0%

: 1345518-18-4
4-(2-{benzyl-[2-(4-benzyloxyphenyl)-ethyl]-amino}-propionyl)phenyl methanesulfonate

: 1173444-33-1
2-{benzyl-[2-(4-benzyloxyphenyl)-ethyl]-amino}-1-(4-hydroxy-phenyl)-propan-1-one

Guidance literature:: 4-(2-{benzyl-[2-(4-benzyloxyphenyl)-ethyl]-amino}-propionyl)phenyl methanesulfonate; With water; potassium hydroxide; In acetone; at 59 ℃; for 2h;

With hydrogenchloride; In water; acetone; at 45 - 50 ℃; pH=7;