N₂-[cis-4-(benzylamino)cyclohexyl]-N₄,N₄,5-trimethylpyridine-2,4-diamine 1-oxide

Base Information

• Chemical Name: N₂-[cis-4-(benzylamino)cyclohexyl]-N₄,N₄,5-trimethylpyridine-2,4-diamine 1-oxide
• CAS No.: 881890-97-7
• Molecular Formula: C₂₁H₃₀N₄O
• Molecular Weight: 354.495

Synonyms:N₂-[cis-4-(benzylamino)cyclohexyl]-N₄,N₄,5-trimethylpyridine-2,4-diamine 1-oxide

Chemical Property of N₂-[cis-4-(benzylamino)cyclohexyl]-N₄,N₄,5-trimethylpyridine-2,4-diamine 1-oxide

Chemical Property:

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Technology Process of N₂-[cis-4-(benzylamino)cyclohexyl]-N₄,N₄,5-trimethylpyridine-2,4-diamine 1-oxide

There total 1 articles about N₂-[cis-4-(benzylamino)cyclohexyl]-N₄,N₄,5-trimethylpyridine-2,4-diamine 1-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cis-N-benzyl-N'-(4-chloro-5-methyl-1-oxidopyridin-2-yl)cyclohexane-1,4-diamine (881890-96-6) + dimethyl amine (124-40-3) → N2-[cis-4-(benzylamino)cyclohexyl]-N4,N4,5-trimethylpyridine-2,4-diamine 1-oxide (881890-97-7)

Guidance literature:

cis-N-benzyl-N'-(4-chloro-5-methyl-1-oxidopyridin-2-yl)cyclohexane-1,4-diamine; dimethyl amine; In methanol; butan-1-ol; at 160 ℃; for 3.5h; Microwave;

With sodium hydrogencarbonate; In methanol; chloroform; water; butan-1-ol;

Reference yield:

N2-[cis-4-(benzylamino)cyclohexyl]-N4,N4,5-trimethylpyridine-2,4-diamine 1-oxide (881890-97-7) → N2-(cis-4-aminocyclohexyl)-N4,N4,5-trimethylpyridine-2,4-diamine (881890-98-8)

Guidance literature:

With cyclohexene; palladium 10% on activated carbon; In isopropyl alcohol; for 76h; Heating / reflux;

upstream raw materials:

cis-N-benzyl-N'-(4-chloro-5-methyl-1-oxidopyridin-2-yl)cyclohexane-1,4-diamine

dimethyl amine

Downstream raw materials:

N₂-(cis-4-aminocyclohexyl)-N₄,N₄,5-trimethylpyridine-2,4-diamine

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