O,O-Diethyl 1-ethoxy-2-methylpropylideneamidothiophosphate

Base Information

• Chemical Name: O,O-Diethyl 1-ethoxy-2-methylpropylideneamidothiophosphate
• CAS No.: 135630-14-7
• Molecular Formula: C₁₀H₂₂NO₃PS
• Molecular Weight: 267.329
• Mol file: 135630-14-7.mol

Synonyms:O,O-Diethyl 1-ethoxy-2-methylpropylideneamidothiophosphate

Chemical Property of O,O-Diethyl 1-ethoxy-2-methylpropylideneamidothiophosphate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of O,O-Diethyl 1-ethoxy-2-methylpropylideneamidothiophosphate

There total 1 articles about O,O-Diethyl 1-ethoxy-2-methylpropylideneamidothiophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 12.0%

ethyl isobutyrimidate hydrochloride (52070-18-5) + diethyl phosphorochloridothioate (2524-04-1) → O,O-diethyl phosphoramidothioate (17321-48-1) + O,O-Diethyl 1-ethoxy-2-methylpropylideneamidothiophosphate (135630-14-7)

Guidance literature:

With triethylamine; In chloroform; at 40 - 45 ℃; for 5h;

Reference yield:

O,O-Diethyl 1-ethoxy-2-methylpropylideneamidothiophosphate (135630-14-7) → O,O-diethyl phosphoramidothioate (17321-48-1) + ISOPROPYLAMIDE (563-83-7) + Ethyl isobutyrate (97-62-1)

Guidance literature:

In 1,4-dioxane; at 55 - 85 ℃; hydrolysis;

upstream raw materials:

ethyl isobutyrimidate hydrochloride

diethyl phosphorochloridothioate

Downstream raw materials:

O,O-diethyl phosphoramidothioate

ISOPROPYLAMIDE

Ethyl isobutyrate