(E,E)-1-dimethoxymethyl-2-(3-(2-(3-(2-phenylmethylsulfanylphenyl)-2-propenylsulfanyl)phenyl)-2-propenylsulfanyl)benzene

Base Information

Chemical Name:(E,E)-1-dimethoxymethyl-2-(3-(2-(3-(2-phenylmethylsulfanylphenyl)-2-propenylsulfanyl)phenyl)-2-propenylsulfanyl)benzene
CAS No.:854280-60-7
Molecular Formula:C₃₄H₃₄O₂S₃
Molecular Weight:570.841
Hs Code.:

Synonyms:(E,E)-1-dimethoxymethyl-2-(3-(2-(3-(2-phenylmethylsulfanylphenyl)-2-propenylsulfanyl)phenyl)-2-propenylsulfanyl)benzene

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Chemical Property of (E,E)-1-dimethoxymethyl-2-(3-(2-(3-(2-phenylmethylsulfanylphenyl)-2-propenylsulfanyl)phenyl)-2-propenylsulfanyl)benzene

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Technology Process of (E,E)-1-dimethoxymethyl-2-(3-(2-(3-(2-phenylmethylsulfanylphenyl)-2-propenylsulfanyl)phenyl)-2-propenylsulfanyl)benzene

There total 11 articles about (E,E)-1-dimethoxymethyl-2-(3-(2-(3-(2-phenylmethylsulfanylphenyl)-2-propenylsulfanyl)phenyl)-2-propenylsulfanyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 854280-58-3
(E,E)-3-(2-(3-(2-benzylsulfanylphenyl)-2-propenylsulfanyl)phenyl)-2-propenol

: 1-(dimethoxymethyl)-2-mercaptobenzene

: 854280-60-7
(E,E)-1-dimethoxymethyl-2-(3-(2-(3-(2-phenylmethylsulfanylphenyl)-2-propenylsulfanyl)phenyl)-2-propenylsulfanyl)benzene

Guidance literature:: With tributylphosphine; di-isopropyl azodicarboxylate; In tetrahydrofuran;
DOI:10.1016/j.tetlet.2005.03.161

Reference yield:

: 854280-53-8
(E)-3-(2-benzylsulfanylphenyl)-2-propenol

: 854280-60-7
(E,E)-1-dimethoxymethyl-2-(3-(2-(3-(2-phenylmethylsulfanylphenyl)-2-propenylsulfanyl)phenyl)-2-propenylsulfanyl)benzene

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / DIAD; PBu₃ / tetrahydrofuran

2: 86 percent / TBAF / tetrahydrofuran / 1.5 h / 20 °C

3: 89 percent / DIAD; PBu₃ / tetrahydrofuran

With tributylphosphine; di-isopropyl azodicarboxylate; tetrabutyl ammonium fluoride; In tetrahydrofuran;
DOI:10.1016/j.tetlet.2005.03.161

Reference yield:

: 854280-52-7
methyl (E)-3-(2-benzylsulfanylphenyl)acrylate

: 854280-60-7
(E,E)-1-dimethoxymethyl-2-(3-(2-(3-(2-phenylmethylsulfanylphenyl)-2-propenylsulfanyl)phenyl)-2-propenylsulfanyl)benzene

Guidance literature:: Multi-step reaction with 4 steps

1: 97 percent / DIBAL-H / CH₂Cl₂ / -78 °C

2: 87 percent / DIAD; PBu₃ / tetrahydrofuran

3: 86 percent / TBAF / tetrahydrofuran / 1.5 h / 20 °C

4: 89 percent / DIAD; PBu₃ / tetrahydrofuran

With tributylphosphine; di-isopropyl azodicarboxylate; tetrabutyl ammonium fluoride; diisobutylaluminium hydride; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tetlet.2005.03.161