(E,E)-3-(2-(3-(2-benzylsulfanylphenyl)-2-propenylsulfanyl)phenyl)-2-propenol

Base Information

Chemical Name:(E,E)-3-(2-(3-(2-benzylsulfanylphenyl)-2-propenylsulfanyl)phenyl)-2-propenol
CAS No.:854280-58-3
Molecular Formula:C₂₅H₂₄OS₂
Molecular Weight:404.597
Hs Code.:

Synonyms:(E,E)-3-(2-(3-(2-benzylsulfanylphenyl)-2-propenylsulfanyl)phenyl)-2-propenol

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Chemical Property of (E,E)-3-(2-(3-(2-benzylsulfanylphenyl)-2-propenylsulfanyl)phenyl)-2-propenol

Chemical Property:

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Technology Process of (E,E)-3-(2-(3-(2-benzylsulfanylphenyl)-2-propenylsulfanyl)phenyl)-2-propenol

There total 10 articles about (E,E)-3-(2-(3-(2-benzylsulfanylphenyl)-2-propenylsulfanyl)phenyl)-2-propenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 854280-57-2
(E,E)-1-tert-butyldiphenylsilyloxy-3-(2-(3-(2-benzylsulfanylphenyl)prop-2-enylsulfanyl)phenyl)-2-propene

: 854280-58-3
(E,E)-3-(2-(3-(2-benzylsulfanylphenyl)-2-propenylsulfanyl)phenyl)-2-propenol

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 1.5h;
DOI:10.1016/j.tetlet.2005.03.161

Reference yield:

: 854280-53-8
(E)-3-(2-benzylsulfanylphenyl)-2-propenol

: 854280-58-3
(E,E)-3-(2-(3-(2-benzylsulfanylphenyl)-2-propenylsulfanyl)phenyl)-2-propenol

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / DIAD; PBu₃ / tetrahydrofuran

2: 86 percent / TBAF / tetrahydrofuran / 1.5 h / 20 °C

With tributylphosphine; di-isopropyl azodicarboxylate; tetrabutyl ammonium fluoride; In tetrahydrofuran;
DOI:10.1016/j.tetlet.2005.03.161

Reference yield:

: 854280-52-7
methyl (E)-3-(2-benzylsulfanylphenyl)acrylate

: 854280-58-3
(E,E)-3-(2-(3-(2-benzylsulfanylphenyl)-2-propenylsulfanyl)phenyl)-2-propenol

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / DIBAL-H / CH₂Cl₂ / -78 °C

2: 87 percent / DIAD; PBu₃ / tetrahydrofuran

3: 86 percent / TBAF / tetrahydrofuran / 1.5 h / 20 °C

With tributylphosphine; di-isopropyl azodicarboxylate; tetrabutyl ammonium fluoride; diisobutylaluminium hydride; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tetlet.2005.03.161