3-vinyl-5,10,15-tris(pentafluorophenyl)corrolatogallium(III) (pyridine)

Base Information

• Chemical Name: 3-vinyl-5,10,15-tris(pentafluorophenyl)corrolatogallium(III) (pyridine)
• CAS No.: 1600520-64-6
• Molecular Formula: C₄₄H₁₅F₁₅GaN₅
• Molecular Weight: 968.336
• Mol file: 1600520-64-6.mol

Synonyms:3-vinyl-5,10,15-tris(pentafluorophenyl)corrolatogallium(III) (pyridine)

Chemical Property of 3-vinyl-5,10,15-tris(pentafluorophenyl)corrolatogallium(III) (pyridine)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-vinyl-5,10,15-tris(pentafluorophenyl)corrolatogallium(III) (pyridine)

There total 1 articles about 3-vinyl-5,10,15-tris(pentafluorophenyl)corrolatogallium(III) (pyridine) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C43H13F15GaN5O (443927-47-7) + Methyltriphenylphosphonium bromide (1779-49-3) → 3-vinyl-5,10,15-tris(pentafluorophenyl)corrolatogallium(III) (pyridine) (1600520-64-6)

Guidance literature:

With sodium hydride; In tetrahydrofuran;

DOI:10.1016/j.ica.2013.09.049

Reference yield: 92.0%

pyridine (110-86-1) + formaldehyd (50-00-0,30525-89-4,61233-19-0) + 4-hydroxy[1]benzopyran-2-one (1076-38-6,92395-12-5) + 3-vinyl-5,10,15-tris(pentafluorophenyl)corrolatogallium(III) (pyridine) (1600520-64-6) → C54H21F15GaN5O3 (1600520-65-7)

Guidance literature:

formaldehyd; 4-hydroxy[1]benzopyran-2-one; 3-vinyl-5,10,15-tris(pentafluorophenyl)corrolatogallium(III) (pyridine); In 1,4-dioxane; for 1h; Reflux;

pyridine; In hexane; ethyl acetate;

DOI:10.1016/j.tet.2013.07.022

Reference yield: 92.0%

C10H8O3 + 3-vinyl-5,10,15-tris(pentafluorophenyl)corrole (1600520-64-6) → C54H21F15GaN5O3 (1600520-65-7)

Guidance literature:

In 1,4-dioxane; Reflux;

DOI:10.1002/open.201402001

upstream raw materials:

C₄₃H₁₃F₁₅GaN₅O

Methyltriphenylphosphonium bromide

Downstream raw materials:

C₅₄H₂₁F₁₅GaN₅O₃

C₅₅H₂₃F₁₅GaN₅O₃

C₅₄H₂₁F₁₅GaN₅O₃

C₅₅H₂₃F₁₅GaN₅O₃