dimesitylphosphine-tris(pentafluorophenyl)borane

Base Information

Chemical Name:dimesitylphosphine-tris(pentafluorophenyl)borane
CAS No.:1070984-70-1
Molecular Formula:C₃₆H₂₃BF₁₅P
Molecular Weight:782.339
Hs Code.:

Synonyms:dimesitylphosphine-tris(pentafluorophenyl)borane

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Chemical Property of dimesitylphosphine-tris(pentafluorophenyl)borane

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Technology Process of dimesitylphosphine-tris(pentafluorophenyl)borane

There total 3 articles about dimesitylphosphine-tris(pentafluorophenyl)borane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1732-66-7
dimesityl phosphine

: 1109-15-5
tris(pentafluorophenyl)borate

: 1070984-70-1
dimesitylphosphine-tris(pentafluorophenyl)borane

Guidance literature:: In pentane; (Ar); std. Schlenk technique; soln. of phosphine in pentane was added tosuspn. of borane in pentane at room temp.; stirred for 2 h; filtered; concd.; cooled to -20°C overnight;
DOI:10.1021/om800339c

Reference yield: 73.0%

: 1070984-62-1
rac-α-(dimesitylphosphino)[3]ferrocenophane

: 1109-15-5
tris(pentafluorophenyl)borate

: 1333-74-0
hydrogen

: 109290-03-1
1,1'-[butane-1,3-diyl]ferrocene

: 1070984-70-1
dimesitylphosphine-tris(pentafluorophenyl)borane

Guidance literature:: In benzene-d6; (Ar); std. Schlenk technique; borane was added to soln. of Fe complex inC6D6; evacuated; H2 was applied (4 h); stirred overnight; treated with S8 for 2 h; chromd. (silica, pentane);
DOI:10.1021/om800339c

Reference yield: 57.0%

: 1070984-66-5
rac-(1-(dimesitylphosphino)ethyl)ferrocene

: 1109-15-5
tris(pentafluorophenyl)borate

: 1333-74-0
hydrogen

: 1-ethylferrocene

: 1070984-70-1
dimesitylphosphine-tris(pentafluorophenyl)borane

Guidance literature:: In benzene-d6; (Ar); std. Schlenk technique; mixt. of Fe complex and borane in C6D6 wasstirred under H2 for 12 h; NMR monitoring; chromd. (pentane);
DOI:10.1021/om800339c