5,10,15,20-tetra(p-tolyl)porphyrinato-iridium(III)-p-bromophenyl

Base Information

Chemical Name:5,10,15,20-tetra(p-tolyl)porphyrinato-iridium(III)-p-bromophenyl
CAS No.:1280227-57-7
Molecular Formula:C₅₄H₄₁BrIrN₄
Molecular Weight:1018.07
Hs Code.:

Synonyms:5,10,15,20-tetra(p-tolyl)porphyrinato-iridium(III)-p-bromophenyl

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Chemical Property of 5,10,15,20-tetra(p-tolyl)porphyrinato-iridium(III)-p-bromophenyl

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Technology Process of 5,10,15,20-tetra(p-tolyl)porphyrinato-iridium(III)-p-bromophenyl

There total 8 articles about 5,10,15,20-tetra(p-tolyl)porphyrinato-iridium(III)-p-bromophenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 872415-81-1
(5,10,15,20-tetrakis(p-tolyl)porphyrinato)carbonyliridium(III) chloride

: 589-87-7
1,4-bromoiodobenzene

: 1280227-57-7
5,10,15,20-tetra(p-tolyl)porphyrinato-iridium(III)-p-bromophenyl

Guidance literature:: With K₂CO₃; In benzene; Ir-complex, IC6H4Br, K2CO3 and benzene were heated in a Teflon-screw-capped tube at 200°C under N2 for 11-19 h; column chromy. on alumina (CH2Cl2/hexane 1/3);
DOI:10.1021/om200251k

Reference yield: 77.0%

: 872415-81-1
(5,10,15,20-tetrakis(p-tolyl)porphyrinato)carbonyliridium(III) chloride

: 589-87-7
1,4-bromoiodobenzene

: 1280227-57-7
5,10,15,20-tetra(p-tolyl)porphyrinato-iridium(III)-p-bromophenyl

: 1319721-19-1
(4-iodophenyl)(5,10,15,20-tetrakis(p-tolyl)porphyrinato)iridium(III)

Guidance literature:: With sodium hydroxide; In benzene; at 150 ℃; for 12h; Inert atmosphere; Darkness;
DOI:10.1021/om200251k

Reference yield: 77.0%

: 872415-81-1
(5,10,15,20-tetrakis(p-tolyl)porphyrinato)carbonyliridium(III) chloride

: 589-87-7
1,4-bromoiodobenzene

: 1280227-57-7
5,10,15,20-tetra(p-tolyl)porphyrinato-iridium(III)-p-bromophenyl

: 1319721-16-8
Ir(ttp)(p-C₆H₄)2(p-I)

: 1,4-bis[ (5,10,15,20-tetrakis(p-tolyl)porphyrinato)iridium(III)] benzene

Guidance literature:: With NaOH; In benzene; Ir-complex, NaOH, 1-bromo-4-iodobenzene and benzene were heated in a Teflon-screw-capped tube at 150°C under N2 for 12 h; column chromy. over alumina with CH2Cl2/hexane (1/2);
DOI:10.1021/om200251k