1,4-bis(trimethylsilyl)-2,5-dihexoxybenzene

Base Information

Chemical Name:1,4-bis(trimethylsilyl)-2,5-dihexoxybenzene
CAS No.:255822-25-4
Molecular Formula:C₂₄H₄₆O₂Si₂
Molecular Weight:422.799
Hs Code.:

Synonyms:1,4-bis(trimethylsilyl)-2,5-dihexoxybenzene

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Chemical Property of 1,4-bis(trimethylsilyl)-2,5-dihexoxybenzene

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Technology Process of 1,4-bis(trimethylsilyl)-2,5-dihexoxybenzene

There total 4 articles about 1,4-bis(trimethylsilyl)-2,5-dihexoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 75-77-4
chloro-trimethyl-silane

: 128424-36-2
2,5-dihexyloxy-1,4-dibromobenzene

: 255822-25-4
1,4-bis(trimethylsilyl)-2,5-dihexoxybenzene

Guidance literature:: chloro-trimethyl-silane; With magnesium; In tetrahydrofuran;

2,5-dihexyloxy-1,4-dibromobenzene; In tetrahydrofuran; at 0 - 20 ℃;
DOI:10.1080/10426509908031635

Reference yield:

: 111-25-1
1-bromo-hexane

: 255822-25-4
1,4-bis(trimethylsilyl)-2,5-dihexoxybenzene

Guidance literature:: Multi-step reaction with 3 steps

1.1: KOH / ethanol / 1 h / 20 °C

1.2: 60 percent / ethanol / 24 h / Heating

2.1: 65 percent / Br₂ / CCl₄ / 20 h / 20 °C

3.1: Mg / tetrahydrofuran

3.2: 80 percent / tetrahydrofuran / 0 - 20 °C

With potassium hydroxide; bromine; magnesium; In tetrahydrofuran; tetrachloromethane; ethanol; 1.1: Metallation / 1.2: Alkylation / 2.1: Bromination / 3.1: Grignard reaction / 3.2: Substitution;
DOI:10.1080/10426509908031635

Reference yield:

: 67399-93-3
1,4-dihexyloxybenzene

: 255822-25-4
1,4-bis(trimethylsilyl)-2,5-dihexoxybenzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: 65 percent / Br₂ / CCl₄ / 20 h / 20 °C

2.1: Mg / tetrahydrofuran

2.2: 80 percent / tetrahydrofuran / 0 - 20 °C

With bromine; magnesium; In tetrahydrofuran; tetrachloromethane; 1.1: Bromination / 2.1: Grignard reaction / 2.2: Substitution;
DOI:10.1080/10426509908031635