(η5-C5Cl5)Mn(CO)3

Base Information

• Chemical Name: (η5-C5Cl5)Mn(CO)3
• CAS No.: 56282-21-4
• Molecular Formula: C₈Cl₅MnO₃
• Molecular Weight: 376.289

Synonyms:(η5-C5Cl5)Mn(CO)3

Chemical Property of (η5-C5Cl5)Mn(CO)3

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

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Technology Process of (η5-C5Cl5)Mn(CO)3

There total 4 articles about (η5-C5Cl5)Mn(CO)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(η1-C5Cl5)Mn(CO)5 (53158-67-1) → dimanganese decacarbonyl (10170-69-1) + pentacarbonylchloromanganese(I) (14100-30-2) + (η5-C5Cl5)Mn(CO)3 (56282-21-4)

Guidance literature:

In further solvent(s); byproducts: CO; Irradiation (UV/VIS); near-UV irradn. (Ar) in alkane solvents at 295K; ratio of Mn(CO)5Cl to product derived from CO loss depends on excitation wavelength, shorter wavelengths favour formation of η5 complex; not isolated, IR;

DOI:10.1021/ja00157a026

Reference yield:

(η1-C5Cl5)Mn(CO)5 (53158-67-1) → pentacarbonylchloromanganese(I) (14100-30-2) + (η5-C5Cl5)Mn(CO)3 (56282-21-4) + (η3-C5Cl5)Mn(CO)4 (123001-82-1)

Guidance literature:

In methyl cyclohexane; byproducts: CO; Irradiation (UV/VIS); near-UV irradn. (Ar) in methylcyclohexane contg. CO at 200K; decrease in the ratio of the CO-loss products to Mn(CO)5Cl as compared to irradn. in absence of CO; not isolated, IR;

DOI:10.1021/ja00157a026

Reference yield:

(η1-C5Cl5)Mn(CO)5 (53158-67-1) → pentacarbonylchloromanganese(I) (14100-30-2) + (η5-C5Cl5)Mn(CO)3 (56282-21-4) + Octachlorbicyclopentadienyliden (6298-65-3)

Guidance literature:

In not given; byproducts: CO, bis(pentachlorocyclopentadienyl); Irradiation (UV/VIS); near-UV irradn. (Ar) in alkane solvents contg. O2 at 295K; not isolated, IR;

DOI:10.1021/ja00157a026

upstream raw materials:

(η1-C5Cl5)Mn(CO)5

Downstream raw materials:

(η5-C5Cl5)Mn(CO)2(PPh3)

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