2-(4-cyano-4-((phenylcarbonothioyl)thio)pentanamido)ethyl 4-(pyren-1-yl)butanoate

Base Information

Chemical Name:2-(4-cyano-4-((phenylcarbonothioyl)thio)pentanamido)ethyl 4-(pyren-1-yl)butanoate
CAS No.:1259437-57-4
Molecular Formula:C₃₅H₃₂N₂O₃S₂
Molecular Weight:592.783
Hs Code.:

Synonyms:2-(4-cyano-4-((phenylcarbonothioyl)thio)pentanamido)ethyl 4-(pyren-1-yl)butanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(4-cyano-4-((phenylcarbonothioyl)thio)pentanamido)ethyl 4-(pyren-1-yl)butanoate

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Technology Process of 2-(4-cyano-4-((phenylcarbonothioyl)thio)pentanamido)ethyl 4-(pyren-1-yl)butanoate

There total 2 articles about 2-(4-cyano-4-((phenylcarbonothioyl)thio)pentanamido)ethyl 4-(pyren-1-yl)butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.3%

: 3443-45-6
1-pyrenebutyric acid

: 2-cyano-5-((2-hydroxyethyl)amino)-5-oxopentan-2-yl benzodithioate

: 1259437-57-4
2-(4-cyano-4-((phenylcarbonothioyl)thio)pentanamido)ethyl 4-(pyren-1-yl)butanoate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In tetrahydrofuran; at 20 ℃;
DOI:10.1021/ma102386j

Reference yield:

: 887764-14-9
dithiobenzoic Acid 1-cyano-1-methyl-4-oxo-4-(2-thioxothiazolidin-3-yl)butyl ester

: 1259437-57-4
2-(4-cyano-4-((phenylcarbonothioyl)thio)pentanamido)ethyl 4-(pyren-1-yl)butanoate

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 20 °C

2: dmap; dicyclohexyl-carbodiimide / tetrahydrofuran / 20 °C

With dmap; dicyclohexyl-carbodiimide; In tetrahydrofuran;
DOI:10.1021/ma102386j