dithiobenzoic Acid 1-cyano-1-methyl-4-oxo-4-(2-thioxothiazolidin-3-yl)butyl ester

Base Information

• Chemical Name: dithiobenzoic Acid 1-cyano-1-methyl-4-oxo-4-(2-thioxothiazolidin-3-yl)butyl ester
• CAS No.: 887764-14-9
• Molecular Formula: C₁₆H₁₆N₂OS₄
• Molecular Weight: 380.58

Synonyms:dithiobenzoic Acid 1-cyano-1-methyl-4-oxo-4-(2-thioxothiazolidin-3-yl)butyl ester

Chemical Property of dithiobenzoic Acid 1-cyano-1-methyl-4-oxo-4-(2-thioxothiazolidin-3-yl)butyl ester

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

Safty Information:

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Technology Process of dithiobenzoic Acid 1-cyano-1-methyl-4-oxo-4-(2-thioxothiazolidin-3-yl)butyl ester

There total 3 articles about dithiobenzoic Acid 1-cyano-1-methyl-4-oxo-4-(2-thioxothiazolidin-3-yl)butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.7%

thiazolidine-2-thione (134469-06-0) + 4-cyano-4-(thiobenzoylthio)pentanoic acid (201611-92-9) → dithiobenzoic Acid 1-cyano-1-methyl-4-oxo-4-(2-thioxothiazolidin-3-yl)butyl ester (887764-14-9)

Guidance literature:

With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 25 ℃; for 6h; Inert atmosphere;

DOI:10.1039/b907061c

Reference yield: 56.0%

bis(thiobenzoyl) disulfide (5873-93-8) + 2-[1-cyano-1-methyl-4-oxo-4-(2-thioxo-thiazolidin-3-yl)-butylazo]-2-methyl-5-oxo-5-(2-thioxothiazolidin-3-yl)-pentanenitrile (870779-03-6) → dithiobenzoic Acid 1-cyano-1-methyl-4-oxo-4-(2-thioxothiazolidin-3-yl)butyl ester (887764-14-9)

Guidance literature:

In ethyl acetate; at 80 ℃; for 6h;

DOI:10.1021/ma400042u

Reference yield:

→ dithiobenzoic Acid 1-cyano-1-methyl-4-oxo-4-(2-thioxothiazolidin-3-yl)butyl ester (887764-14-9)

Guidance literature:

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dimethyl sulfoxide; at 20 ℃; for 2h;

upstream raw materials:

thiazolidine-2-thione

4-cyano-4-(thiobenzoylthio)pentanoic acid

bis(thiobenzoyl) disulfide

2-[1-cyano-1-methyl-4-oxo-4-(2-thioxo-thiazolidin-3-yl)-butylazo]-2-methyl-5-oxo-5-(2-thioxothiazolidin-3-yl)-pentanenitrile

Downstream raw materials:

2-(4-cyano-4-((phenylcarbonothioyl)thio)pentanamido)ethyl 4-(pyren-1-yl)butanoate

5-(bis(2-hydroxyethyl)amino)-2-cyano-5-oxopentan-2-yl benzodithioate

C₂₃H₂₈Br₂N₂O₅S₂

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