1-benzyl-4-(((1-(1-benzyl-1H-1,2,3-triazol-4-yl)-2-(4-(phenylsulfonyl)phenyl)propan-2-yl)oxy)methyl)-1H-1,2,3-triazole

Base Information

Chemical Name:1-benzyl-4-(((1-(1-benzyl-1H-1,2,3-triazol-4-yl)-2-(4-(phenylsulfonyl)phenyl)propan-2-yl)oxy)methyl)-1H-1,2,3-triazole
CAS No.:1621085-10-6
Molecular Formula:C₃₄H₃₂N₆O₃S
Molecular Weight:604.732
Hs Code.:

Synonyms:1-benzyl-4-(((1-(1-benzyl-1H-1,2,3-triazol-4-yl)-2-(4-(phenylsulfonyl)phenyl)propan-2-yl)oxy)methyl)-1H-1,2,3-triazole

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Chemical Property of 1-benzyl-4-(((1-(1-benzyl-1H-1,2,3-triazol-4-yl)-2-(4-(phenylsulfonyl)phenyl)propan-2-yl)oxy)methyl)-1H-1,2,3-triazole

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Technology Process of 1-benzyl-4-(((1-(1-benzyl-1H-1,2,3-triazol-4-yl)-2-(4-(phenylsulfonyl)phenyl)propan-2-yl)oxy)methyl)-1H-1,2,3-triazole

There total 5 articles about 1-benzyl-4-(((1-(1-benzyl-1H-1,2,3-triazol-4-yl)-2-(4-(phenylsulfonyl)phenyl)propan-2-yl)oxy)methyl)-1H-1,2,3-triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1621085-08-2
1-benzyl-4-(2-(4-(phenylsulfonyl)phenyl)-2-(prop-2-yn-1-yloxy)propyl)-1H-1,2,3-triazole

: 622-79-7
benzyl azide

: 1621085-10-6
1-benzyl-4-(((1-(1-benzyl-1H-1,2,3-triazol-4-yl)-2-(4-(phenylsulfonyl)phenyl)propan-2-yl)oxy)methyl)-1H-1,2,3-triazole

Guidance literature:: With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In water; tert-butyl alcohol; at 25 - 30 ℃; for 0.5h; Sonication; Green chemistry;
DOI:10.1016/j.ejmech.2014.07.042

Reference yield: 86.0%

: 1621085-12-8
1-(phenylsulfonyl)-4-(2-(prop-2-yn-1-yloxy)pent-4-yn-2-yl)benzene

: 622-79-7
benzyl azide

: 1621085-10-6
1-benzyl-4-(((1-(1-benzyl-1H-1,2,3-triazol-4-yl)-2-(4-(phenylsulfonyl)phenyl)propan-2-yl)oxy)methyl)-1H-1,2,3-triazole

Guidance literature:: With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In water; tert-butyl alcohol; at 25 - 30 ℃; for 0.5h; Sonication; Green chemistry;
DOI:10.1016/j.ejmech.2014.07.042

Reference yield:

: 65085-83-8
4'-(phenylsulfonyl)acetophenone

: 1621085-10-6
1-benzyl-4-(((1-(1-benzyl-1H-1,2,3-triazol-4-yl)-2-(4-(phenylsulfonyl)phenyl)propan-2-yl)oxy)methyl)-1H-1,2,3-triazole

Guidance literature:: Multi-step reaction with 3 steps

1.1: zinc; zinc dibromide / tetrahydrofuran / 1.5 h / 25 - 30 °C / Sonication

2.1: sodium hydride / N,N-dimethyl-formamide / -20 °C

2.2: 0.5 h / -20 °C / Sonication

3.1: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; tert-butyl alcohol / 0.5 h / 25 - 30 °C / Sonication; Green chemistry

With copper(ll) sulfate pentahydrate; sodium hydride; sodium L-ascorbate; zinc dibromide; zinc; In tetrahydrofuran; water; N,N-dimethyl-formamide; tert-butyl alcohol; 1.1: |Barbier Coupling Reaction;
DOI:10.1016/j.ejmech.2014.07.042