4-Allyl-2-iodophenyl methoxymethyl ether

Base Information

Chemical Name:4-Allyl-2-iodophenyl methoxymethyl ether
CAS No.:163125-71-1
Molecular Formula:C₁₁H₁₃IO₂
Molecular Weight:304.128
Hs Code.:

Synonyms:4-Allyl-2-iodophenyl methoxymethyl ether

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Chemical Property of 4-Allyl-2-iodophenyl methoxymethyl ether

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Technology Process of 4-Allyl-2-iodophenyl methoxymethyl ether

There total 1 articles about 4-Allyl-2-iodophenyl methoxymethyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 70482-71-2
1-allyl-4-(methoxymethoxy)benzene

: 163125-71-1
4-Allyl-2-iodophenyl methoxymethyl ether

Guidance literature:: With iodine; tert.-butyl lithium; In tetrahydrofuran; hexane; 1.) -78 deg C, 2 h, 2.) -78 deg C, 30 min;
DOI:10.1021/jo00111a052

Reference yield: 71.0%

: 97-53-0
4-allylguaiacol

: 163125-71-1
4-Allyl-2-iodophenyl methoxymethyl ether

: C₂₁H₂₄O₄

Guidance literature:: With t-butyl malonate; caesium carbonate; copper(l) chloride; In 1,4-dioxane; 1-methyl-pyrrolidin-2-one; at 80 ℃;
DOI:10.1021/acsinfecdis.0c00523

Reference yield:

: 163125-71-1
4-Allyl-2-iodophenyl methoxymethyl ether

: C₁₉H₂₀O₃

Guidance literature:: Multi-step reaction with 2 steps

1: copper(l) chloride; t-butyl malonate; caesium carbonate / 1-methyl-pyrrolidin-2-one; 1,4-dioxane / 80 °C

2: hydrogenchloride / water; methanol

With hydrogenchloride; t-butyl malonate; caesium carbonate; copper(l) chloride; In 1,4-dioxane; 1-methyl-pyrrolidin-2-one; methanol; water; 1: |Ullmann Condensation;
DOI:10.1021/acsinfecdis.0c00523