1-(Methoxymethoxy)-4-(2-propen-1-YL)benzene

Base Information

Chemical Name:1-(Methoxymethoxy)-4-(2-propen-1-YL)benzene
CAS No.:70482-71-2
Molecular Formula:C11H14O2
Molecular Weight:178.231
Hs Code.:
DSSTox Substance ID:DTXSID10437449
Wikidata:Q72490244
Mol file:70482-71-2.mol

Synonyms:70482-71-2;1-(METHOXYMETHOXY)-4-(2-PROPEN-1-YL)BENZENE;1-(methoxymethoxy)-4-prop-2-enylbenzene;SCHEMBL10484099;DTXSID10437449;1-(Methoxymethoxy)-4-(prop-2-en-1-yl)benzene

Suppliers and Price of 1-(Methoxymethoxy)-4-(2-propen-1-YL)benzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 8 raw suppliers

Chemical Property of 1-(Methoxymethoxy)-4-(2-propen-1-YL)benzene

Chemical Property:

PSA：18.46000
Density:0.986
LogP:2.39780
XLogP3:2.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:5
Exact Mass:178.099379685
Heavy Atom Count:13
Complexity:137

Purity/Quality:: 98%min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COCOC1=CC=C(C=C1)CC=C

Technology Process of 1-(Methoxymethoxy)-4-(2-propen-1-YL)benzene

There total 5 articles about 1-(Methoxymethoxy)-4-(2-propen-1-YL)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 25458-45-1
p-methoxymethoxybromobenzene

: 106-95-6
allyl bromide

: 70482-71-2
1-allyl-4-(methoxymethoxy)benzene

Guidance literature:: p-methoxymethoxybromobenzene; With magnesium; In tetrahydrofuran;

allyl bromide; In tetrahydrofuran; at 20 ℃; for 2.5h; Reflux;
DOI:10.1016/j.tetlet.2020.152229

Reference yield: 89.0%

: 501-92-8
4-(prop-2-enyl)phenol

: 107-30-2
chloromethyl methyl ether

: 70482-71-2
1-allyl-4-(methoxymethoxy)benzene

Guidance literature:: With sodium hydride; In tetrahydrofuran; 1.) r.t., 1 h, 2.) r.t., 12 h;
DOI:10.1021/jo00111a052

Reference yield:

: 106-41-2
4-bromo-phenol

: 70482-71-2
1-allyl-4-(methoxymethoxy)benzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.25 h / 0 °C / Inert atmosphere

1.2: 1.17 h / 0 °C / Inert atmosphere

2.1: magnesium / tetrahydrofuran

2.2: 2.5 h / 20 °C / Reflux

With sodium hydride; magnesium; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2020.152229