N,N’,N″-[2,2′,2″-nitrilotris(ethane-2,1-diyl)]tris(2,4,6-tri-methylbenzenesulfonamide)

Base Information

Chemical Name:N,N’,N″-[2,2′,2″-nitrilotris(ethane-2,1-diyl)]tris(2,4,6-tri-methylbenzenesulfonamide)
CAS No.:1311297-64-9
Molecular Formula:C₃₃H₄₈N₄O₆S₃
Molecular Weight:692.965
Hs Code.:

Synonyms:N,N’,N″-[2,2′,2″-nitrilotris(ethane-2,1-diyl)]tris(2,4,6-tri-methylbenzenesulfonamide)

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Chemical Property of N,N’,N″-[2,2′,2″-nitrilotris(ethane-2,1-diyl)]tris(2,4,6-tri-methylbenzenesulfonamide)

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Technology Process of N,N’,N″-[2,2′,2″-nitrilotris(ethane-2,1-diyl)]tris(2,4,6-tri-methylbenzenesulfonamide)

There total 1 articles about N,N’,N″-[2,2′,2″-nitrilotris(ethane-2,1-diyl)]tris(2,4,6-tri-methylbenzenesulfonamide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 773-64-8
2-mesitylenesulphonyl chloride

: 4097-89-6
2,2',2''-triaminotriethylamine

: 1311297-64-9
N,N’,N″-[2,2′,2″-nitrilotris(ethane-2,1-diyl)]tris(2,4,6-tri-methylbenzenesulfonamide)

Guidance literature:: With sodium hydroxide; In diethyl ether; water; at 20 ℃; Inert atmosphere;
DOI:10.1021/ja203458d

Reference yield: 94.0%

: 1311297-64-9
N,N’,N″-[2,2′,2″-nitrilotris(ethane-2,1-diyl)]tris(2,4,6-tri-methylbenzenesulfonamide)

: 10581-12-1
tetramethyl ammonium acetate

: 1834-30-6,2140-52-5,3094-87-9
iron(II) acetate

: NMe₄[Fe^II(N,N’,N’’-[2,2’,2’’-nitrilotris(ethane-2,1-diyl)]tris(2,4,6-trimethylbenzenesulfonamido))]

Guidance literature:: N,N’,N″-[2,2′,2″-nitrilotris(ethane-2,1-diyl)]tris(2,4,6-tri-methylbenzenesulfonamide); With sodium hydride; In N,N-dimethyl acetamide; at 20 ℃; Inert atmosphere;

tetramethyl ammonium acetate; iron(II) acetate; In N,N-dimethyl acetamide; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1039/c2sc21400h

Reference yield: 90.0%

: 1311297-64-9
N,N’,N″-[2,2′,2″-nitrilotris(ethane-2,1-diyl)]tris(2,4,6-tri-methylbenzenesulfonamide)

: 10581-12-1
tetramethyl ammonium acetate

: 638-38-0,993-02-2,2180-18-9,15411-95-7,22981-23-3,27004-39-3
manganese(II) acetate

: 1311309-91-7
[NMe₄][Mn(II)(N,N',N''-[2,2',2''-nitrilotris(ethane-2,1-diyl)]tris(2,4,6-trimethylbenzenesulfonamido)]

Guidance literature:: With NaH; In N,N-dimethyl acetamide; soln. ligand in DMA was treated with 3 equiv. NaH followed by addn. Mn(OAc)2;
DOI:10.1021/ja203458d