morpholinium 4-cyano-1-oxo-2,5,6,7-tetrahydro-1H-cyclopenta[c]pyridine-3-thiolate

Base Information

• Chemical Name: morpholinium 4-cyano-1-oxo-2,5,6,7-tetrahydro-1H-cyclopenta[c]pyridine-3-thiolate
• CAS No.: 1095141-84-6
• Molecular Formula: C₄H₉NO*C₉H₈N₂OS
• Molecular Weight: 279.363

Synonyms:morpholinium 4-cyano-1-oxo-2,5,6,7-tetrahydro-1H-cyclopenta[c]pyridine-3-thiolate

Chemical Property of morpholinium 4-cyano-1-oxo-2,5,6,7-tetrahydro-1H-cyclopenta[c]pyridine-3-thiolate

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Technology Process of morpholinium 4-cyano-1-oxo-2,5,6,7-tetrahydro-1H-cyclopenta[c]pyridine-3-thiolate

There total 1 articles about morpholinium 4-cyano-1-oxo-2,5,6,7-tetrahydro-1H-cyclopenta[c]pyridine-3-thiolate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

Cyanothioacetamide (7357-70-2) + ethyl 2-(N-morpholinyl)cyclopent-1-ene-1-carboxylate (292165-55-0) → morpholinium 4-cyano-1-oxo-2,5,6,7-tetrahydro-1H-cyclopenta[c]pyridine-3-thiolate (1095141-84-6)

Guidance literature:

In ethanol; at 20 ℃; for 5h;

DOI:10.1007/s00706-007-0784-1

Reference yield: 90.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + morpholinium 4-cyano-1-oxo-2,5,6,7-tetrahydro-1H-cyclopenta[c]pyridine-3-thiolate (1095141-84-6) + aniline (62-53-3) → 6-oxo-3-phenyl-3,4,6,7,8,9-2H-cyclopenta[g]pyrido[2,1-b][1,3,5]thiadiazine-10-carbonitrile (1095141-87-9)

Guidance literature:

In ethanol; water; at 25 ℃; for 5h;

DOI:10.1007/s00706-007-0784-1

Reference yield: 88.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + morpholinium 4-cyano-1-oxo-2,5,6,7-tetrahydro-1H-cyclopenta[c]pyridine-3-thiolate (1095141-84-6) + p-toluidine (106-49-0,12221-03-3) → 3-(4-methylphenyl)-6-oxo-3-phenyl-3,4,6,7,8,9-2H-cyclopenta[g]pyrido[2,1-b][1,3,5]thiadiazine-10-carbonitrile (1095141-89-1)

Guidance literature:

In ethanol; water; at 25 ℃; for 5h;

DOI:10.1007/s00706-007-0784-1

upstream raw materials:

Cyanothioacetamide

ethyl 2-(N-morpholinyl)cyclopent-1-ene-1-carboxylate

Downstream raw materials:

3-(4-methylphenyl)-6-oxo-3-phenyl-3,4,6,7,8,9-2H-cyclopenta[g]pyrido[2,1-b][1,3,5]thiadiazine-10-carbonitrile

3-(4-chlorophenyl)-6-oxo-3-phenyl-3,4,6,7,8,9-2H-cyclopenta[g]pyrido[2,1-b][1,3,5]thiadiazine-10-carbonitrile

6-oxo-3-phenyl-3,4,6,7,8,9-2H-cyclopenta[g]pyrido[2,1-b][1,3,5]thiadiazine-10-carbonitrile

3-(4-fluorophenyl)-6-oxo-3-phenyl-3,4,6,7,8,9-2H-cyclopenta[g]pyrido[2,1-b][1,3,5]thiadiazine-10-carbonitrile

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