(1S,2R)-(-)-2-[N-(3’,5’-di-tert-butylsalicylidene)amino]-1,2-diphenylethanol

Base Information

Chemical Name:(1S,2R)-(-)-2-[N-(3’,5’-di-tert-butylsalicylidene)amino]-1,2-diphenylethanol
CAS No.:164021-74-3
Molecular Formula:C₂₉H₃₅NO₂
Molecular Weight:429.602
Hs Code.:

Synonyms:(1S,2R)-(-)-2-[N-(3’,5’-di-tert-butylsalicylidene)amino]-1,2-diphenylethanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S,2R)-(-)-2-[N-(3’,5’-di-tert-butylsalicylidene)amino]-1,2-diphenylethanol

Chemical Property:

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Technology Process of (1S,2R)-(-)-2-[N-(3’,5’-di-tert-butylsalicylidene)amino]-1,2-diphenylethanol

There total 1 articles about (1S,2R)-(-)-2-[N-(3’,5’-di-tert-butylsalicylidene)amino]-1,2-diphenylethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 23364-44-5
(1S,2R)-2-Amino-1,2-diphenylethanol

: 37942-07-7
3,5-di-tert-butyl-2-hydroxybenzaldehyde

: 164021-74-3
(1S,2R)-(-)-2-[N-(3’,5’-di-tert-butylsalicylidene)amino]-1,2-diphenylethanol

Guidance literature:: With sodium sulfate; In methanol; at 20 ℃; for 15h;
DOI:10.1016/j.molcata.2012.04.014

Reference yield:

: 622-38-8
Ethyl phenyl sulfide

: 164021-74-3
(1S,2R)-(-)-2-[N-(3’,5’-di-tert-butylsalicylidene)amino]-1,2-diphenylethanol

: 599-70-2
ethyl phenyl sulfone

: 51207-25-1
(R)-ethyl phenyl sulfoxide

: 4170-80-3,51207-25-1,67529-33-3,104113-36-2
(S)-(-)-ethylphenylsulfoxide

Guidance literature:: With titanium(IV) isopropylate; dihydrogen peroxide; In dichloromethane; water; at 0 ℃; for 10h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1016/j.molcata.2012.04.014

Reference yield:

: 371-15-3
p-fluorothioanisole

: 164021-74-3
(1S,2R)-(-)-2-[N-(3’,5’-di-tert-butylsalicylidene)amino]-1,2-diphenylethanol

: 455-15-2
1-(methylsufonyl)-4-fluorobenzene

: 658-14-0,139696-90-5
R-(-)-4-fluoro phenyl methyl sulfoxide

: 175911-67-8
S-(+)-4-fluoro phenyl methyl sulfoxide

Guidance literature:: With titanium(IV) isopropylate; dihydrogen peroxide; In dichloromethane; water; at 0 ℃; for 10h; optical yield given as %ee; enantiospecific reaction; Inert atmosphere;
DOI:10.1016/j.molcata.2012.04.014