2-(4-chlorophenyl)-3-(2,4-dichlorophenyl)-1-(4-methoxyphenyl)-1-propanone

Base Information

• Chemical Name: 2-(4-chlorophenyl)-3-(2,4-dichlorophenyl)-1-(4-methoxyphenyl)-1-propanone
• CAS No.: 145192-06-9
• Molecular Formula: C₂₂H₁₇Cl₃O₂
• Molecular Weight: 419.735

Synonyms:2-(4-chlorophenyl)-3-(2,4-dichlorophenyl)-1-(4-methoxyphenyl)-1-propanone

Chemical Property of 2-(4-chlorophenyl)-3-(2,4-dichlorophenyl)-1-(4-methoxyphenyl)-1-propanone

Chemical Property:

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Technology Process of 2-(4-chlorophenyl)-3-(2,4-dichlorophenyl)-1-(4-methoxyphenyl)-1-propanone

There total 3 articles about 2-(4-chlorophenyl)-3-(2,4-dichlorophenyl)-1-(4-methoxyphenyl)-1-propanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.9%

2-(4-chlorophenyl)-1-(4-methoxyphenyl)ethanone (52578-11-7) + 2,4-Dichlorobenzyl chloride (94-99-5) → 2-(4-chlorophenyl)-3-(2,4-dichlorophenyl)-1-(4-methoxyphenyl)-1-propanone (145192-06-9)

Guidance literature:

With sodium hydride; In tetrahydrofuran; for 1h; Ambient temperature;

DOI:10.1016/0223-5234(92)90183-2

Reference yield:

methoxybenzene (100-66-3) → 2-(4-chlorophenyl)-3-(2,4-dichlorophenyl)-1-(4-methoxyphenyl)-1-propanone (145192-06-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 78 percent / AlCl₃ / CH₂Cl₂ / 1 h / Ambient temperature

2: 98.9 percent / NaH / tetrahydrofuran / 1 h / Ambient temperature

With aluminium trichloride; sodium hydride; In tetrahydrofuran; dichloromethane;

DOI:10.1016/0223-5234(92)90183-2

Reference yield:

4-chlorophenacetyl chloride (25026-34-0) → 2-(4-chlorophenyl)-3-(2,4-dichlorophenyl)-1-(4-methoxyphenyl)-1-propanone (145192-06-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 78 percent / AlCl₃ / CH₂Cl₂ / 1 h / Ambient temperature

2: 98.9 percent / NaH / tetrahydrofuran / 1 h / Ambient temperature

With aluminium trichloride; sodium hydride; In tetrahydrofuran; dichloromethane;

DOI:10.1016/0223-5234(92)90183-2

upstream raw materials:

2-(4-chlorophenyl)-1-(4-methoxyphenyl)ethanone

2,4-Dichlorobenzyl chloride

methoxybenzene

4-chlorophenacetyl chloride

Downstream raw materials:

2-(4-Chloro-phenyl)-3-(2,4-dichloro-phenyl)-1-(4-methoxy-phenyl)-propan-1-ol

1-[2-(4-chlorophenyl)-3-(2,4-dichlorophenyl)-1-(4-methoxyphenyl)propyl]-1H-imidazole

4-[2-(4-Chloro-phenyl)-3-(2,4-dichloro-phenyl)-1-(4-methoxy-phenyl)-propyl]-4H-[1,2,4]triazole

1-[2-(4-Chloro-phenyl)-3-(2,4-dichloro-phenyl)-1-(4-methoxy-phenyl)-propyl]-1H-[1,2,4]triazole

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