(4-chlorophenyl)(1,1-difluoro-2-(4-isopropylcyclohex-1-enyl)ethyl)sulfane

Base Information

Chemical Name:(4-chlorophenyl)(1,1-difluoro-2-(4-isopropylcyclohex-1-enyl)ethyl)sulfane
CAS No.:1563062-79-2
Molecular Formula:C₁₇H₂₁ClF₂S
Molecular Weight:330.87
Hs Code.:

Synonyms:(4-chlorophenyl)(1,1-difluoro-2-(4-isopropylcyclohex-1-enyl)ethyl)sulfane

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Chemical Property of (4-chlorophenyl)(1,1-difluoro-2-(4-isopropylcyclohex-1-enyl)ethyl)sulfane

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Technology Process of (4-chlorophenyl)(1,1-difluoro-2-(4-isopropylcyclohex-1-enyl)ethyl)sulfane

There total 3 articles about (4-chlorophenyl)(1,1-difluoro-2-(4-isopropylcyclohex-1-enyl)ethyl)sulfane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 10408-16-9
[3.1.0]hexane, 4-methylene-1-(1-methylethyl)bicyclo

: 1563062-31-6
ethyl ({[(4-chlorophenyl)sulfanyl]difluoromethyl}sulfanyl)methanethioate

: 1563062-79-2
(4-chlorophenyl)(1,1-difluoro-2-(4-isopropylcyclohex-1-enyl)ethyl)sulfane

Guidance literature:: [3.1.0]hexane, 4-methylene-1-(1-methylethyl)bicyclo; ethyl ({[(4-chlorophenyl)sulfanyl]difluoromethyl}sulfanyl)methanethioate; With dilauryl peroxide; In ethyl acetate; Reflux; Inert atmosphere;

With hypophosphorous acid; triethylamine; In 1,4-dioxane; water; ethyl acetate; for 0.0833333h; Inert atmosphere; Reflux;

With 2,2'-azobis(isobutyronitrile); In 1,4-dioxane; water; ethyl acetate; Inert atmosphere;
DOI:10.1021/ol5002939

Reference yield:

: 18803-44-6
sodium p-chlorothiophenolate

: 1563062-79-2
(4-chlorophenyl)(1,1-difluoro-2-(4-isopropylcyclohex-1-enyl)ethyl)sulfane

Guidance literature:: Multi-step reaction with 4 steps

1.1: 1,4-dioxane / 4 h / Reflux; Inert atmosphere

2.1: oxalyl dichloride; N,N-dimethyl-formamide / 1,4-dioxane; dichloromethane / Inert atmosphere

3.1: 1,4-dioxane; dichloromethane; cyclohexane / 6 h / 0 °C / Inert atmosphere

3.2: 12 h / Irradiation; Reflux; Inert atmosphere

4.1: dilauryl peroxide / ethyl acetate / Reflux; Inert atmosphere

4.2: 0.08 h / Inert atmosphere; Reflux

4.3: Inert atmosphere

With oxalyl dichloride; dilauryl peroxide; N,N-dimethyl-formamide; In 1,4-dioxane; dichloromethane; cyclohexane; ethyl acetate;
DOI:10.1021/ol5002939

Reference yield:

: 16503-81-4
2-((4-chlorophenyl)thio)-2,2-difluoroacetic acid

: 1563062-79-2
(4-chlorophenyl)(1,1-difluoro-2-(4-isopropylcyclohex-1-enyl)ethyl)sulfane

Guidance literature:: Multi-step reaction with 3 steps

1.1: oxalyl dichloride; N,N-dimethyl-formamide / 1,4-dioxane; dichloromethane / Inert atmosphere

2.1: 1,4-dioxane; dichloromethane; cyclohexane / 6 h / 0 °C / Inert atmosphere

2.2: 12 h / Irradiation; Reflux; Inert atmosphere

3.1: dilauryl peroxide / ethyl acetate / Reflux; Inert atmosphere

3.2: 0.08 h / Inert atmosphere; Reflux

3.3: Inert atmosphere

With oxalyl dichloride; dilauryl peroxide; N,N-dimethyl-formamide; In 1,4-dioxane; dichloromethane; cyclohexane; ethyl acetate;
DOI:10.1021/ol5002939