ethyl ({[(4-chlorophenyl)sulfanyl]difluoromethyl}sulfanyl)methanethioate

Base Information

Chemical Name:ethyl ({[(4-chlorophenyl)sulfanyl]difluoromethyl}sulfanyl)methanethioate
CAS No.:1563062-31-6
Molecular Formula:C₁₀H₉ClF₂OS₃
Molecular Weight:314.829
Hs Code.:

Synonyms:ethyl ({[(4-chlorophenyl)sulfanyl]difluoromethyl}sulfanyl)methanethioate

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Chemical Property of ethyl ({[(4-chlorophenyl)sulfanyl]difluoromethyl}sulfanyl)methanethioate

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Technology Process of ethyl ({[(4-chlorophenyl)sulfanyl]difluoromethyl}sulfanyl)methanethioate

There total 3 articles about ethyl ({[(4-chlorophenyl)sulfanyl]difluoromethyl}sulfanyl)methanethioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 140-89-6
potassium ethyl xanthogenate

: 676316-30-6
4-chlorophenylthiodifluoroacetic acid chloride

: 1563062-31-6
ethyl ({[(4-chlorophenyl)sulfanyl]difluoromethyl}sulfanyl)methanethioate

Guidance literature:: potassium ethyl xanthogenate; 4-chlorophenylthiodifluoroacetic acid chloride; In 1,4-dioxane; dichloromethane; cyclohexane; at 0 ℃; for 6h; Inert atmosphere;

In 1,4-dioxane; dichloromethane; cyclohexane; for 12h; Irradiation; Reflux; Inert atmosphere;
DOI:10.1021/ol5002939

Reference yield:

: 18803-44-6
sodium p-chlorothiophenolate

: 1563062-31-6
ethyl ({[(4-chlorophenyl)sulfanyl]difluoromethyl}sulfanyl)methanethioate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1,4-dioxane / 4 h / Reflux; Inert atmosphere

2.1: oxalyl dichloride; N,N-dimethyl-formamide / 1,4-dioxane; dichloromethane / Inert atmosphere

3.1: 1,4-dioxane; dichloromethane; cyclohexane / 6 h / 0 °C / Inert atmosphere

3.2: 12 h / Irradiation; Reflux; Inert atmosphere

With oxalyl dichloride; N,N-dimethyl-formamide; In 1,4-dioxane; dichloromethane; cyclohexane;
DOI:10.1021/ol5002939

Reference yield:

: 16503-81-4
2-((4-chlorophenyl)thio)-2,2-difluoroacetic acid

: 1563062-31-6
ethyl ({[(4-chlorophenyl)sulfanyl]difluoromethyl}sulfanyl)methanethioate

Guidance literature:: Multi-step reaction with 2 steps

1.1: oxalyl dichloride; N,N-dimethyl-formamide / 1,4-dioxane; dichloromethane / Inert atmosphere

2.1: 1,4-dioxane; dichloromethane; cyclohexane / 6 h / 0 °C / Inert atmosphere

2.2: 12 h / Irradiation; Reflux; Inert atmosphere

With oxalyl dichloride; N,N-dimethyl-formamide; In 1,4-dioxane; dichloromethane; cyclohexane;
DOI:10.1021/ol5002939