Technology Process of C50H51O14P
There total 6 articles about C50H51O14P which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
N-iodo-succinimide; trifluorormethanesulfonic acid;
In
dichloromethane;
at 0 ℃;
for 3h;
Inert atmosphere;
Molecular sieve;
DOI:10.1002/anie.201210176
- Guidance literature:
-
Multi-step reaction with 5 steps
1: pyridine / 0 - 80 °C / Inert atmosphere
2: pyridine / 0 - 20 °C / Inert atmosphere
3: toluene-4-sulfonic acid / dichloromethane; methanol / 20 °C / Inert atmosphere
4: pyridine / dichloromethane / 20 °C / Inert atmosphere
5: N-iodo-succinimide; trifluorormethanesulfonic acid / dichloromethane / 3 h / 0 °C / Inert atmosphere; Molecular sieve
With
pyridine; N-iodo-succinimide; trifluorormethanesulfonic acid; toluene-4-sulfonic acid;
In
methanol; dichloromethane;
DOI:10.1002/anie.201210176
- Guidance literature:
-
Multi-step reaction with 3 steps
1: toluene-4-sulfonic acid / dichloromethane; methanol / 20 °C / Inert atmosphere
2: pyridine / dichloromethane / 20 °C / Inert atmosphere
3: N-iodo-succinimide; trifluorormethanesulfonic acid / dichloromethane / 3 h / 0 °C / Inert atmosphere; Molecular sieve
With
pyridine; N-iodo-succinimide; trifluorormethanesulfonic acid; toluene-4-sulfonic acid;
In
methanol; dichloromethane;
DOI:10.1002/anie.201210176