methyl Δ16-3α-acetoxy-6α-ethyl-7α-(3'-iodobenozyl)oxy-5β-cholan-24-oate

Base Information

Chemical Name:methyl Δ16-3α-acetoxy-6α-ethyl-7α-(3'-iodobenozyl)oxy-5β-cholan-24-oate
CAS No.:1227612-54-5
Molecular Formula:C₃₆H₄₉IO₆
Molecular Weight:704.686
Hs Code.:

Synonyms:methyl Δ16-3α-acetoxy-6α-ethyl-7α-(3'-iodobenozyl)oxy-5β-cholan-24-oate

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Chemical Property of methyl Δ16-3α-acetoxy-6α-ethyl-7α-(3'-iodobenozyl)oxy-5β-cholan-24-oate

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Technology Process of methyl Δ16-3α-acetoxy-6α-ethyl-7α-(3'-iodobenozyl)oxy-5β-cholan-24-oate

There total 5 articles about methyl Δ16-3α-acetoxy-6α-ethyl-7α-(3'-iodobenozyl)oxy-5β-cholan-24-oate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1227612-53-4
methyl 3α-acetoxy-6α-ethyl-7α-(3'-iodobenozyl)oxy-17α-chloro-5β-cholan-24-oate

: 1227612-54-5
methyl Δ16-3α-acetoxy-6α-ethyl-7α-(3'-iodobenozyl)oxy-5β-cholan-24-oate

Guidance literature:: With pyridine; Reflux;

Reference yield:

: 1227612-51-2
methyl 3α-acetoxy-7α-hydroxy-6α-ethyl-5β-cholan-24-oate

: 1227612-54-5
methyl Δ16-3α-acetoxy-6α-ethyl-7α-(3'-iodobenozyl)oxy-5β-cholan-24-oate

Guidance literature:: Multi-step reaction with 3 steps

1: calcium hydride; N-benzyl-N,N,N-triethylammonium chloride / toluene / 48 h / Reflux

2: (Dichloroiodo)benzene; tert-butyl alcohol / dichloromethane / 1 h / 0 °C / Photolysis; Inert atmosphere

3: pyridine / Reflux

With pyridine; calcium hydride; (Dichloroiodo)benzene; N-benzyl-N,N,N-triethylammonium chloride; tert-butyl alcohol; In dichloromethane; toluene;
DOI:10.1021/ml200256d

Reference yield:

: 1227612-52-3
methyl 3α-acetoxy-6α-ethyl-7α-(3'-iodobenozyl)oxy-5β-cholan-24-oate

: 1227612-54-5
methyl Δ16-3α-acetoxy-6α-ethyl-7α-(3'-iodobenozyl)oxy-5β-cholan-24-oate

Guidance literature:: Multi-step reaction with 2 steps

1: (Dichloroiodo)benzene; tert-butyl alcohol / dichloromethane / 1 h / 0 °C / Photolysis; Inert atmosphere

2: pyridine / Reflux

With pyridine; (Dichloroiodo)benzene; tert-butyl alcohol; In dichloromethane;
DOI:10.1021/ml200256d