1-(3-Nitrophenyl)-1h-tetrazol-5-amine

Base Information

Chemical Name:1-(3-Nitrophenyl)-1h-tetrazol-5-amine
CAS No.:5467-77-6
Molecular Formula:C7H6N6O2
Molecular Weight:206.1615
Hs Code.:
NSC Number:25412
DSSTox Substance ID:DTXSID70282316
Nikkaji Number:J2.964.389J
Wikidata:Q82016557
ChEMBL ID:CHEMBL1884445

Synonyms:1-(3-nitrophenyl)tetrazol-5-amine;5467-77-6;MLS002639054;1-(3-nitrophenyl)-1h-tetrazol-5-amine;NSC25412;CHEMBL1884445;DTXSID70282316;HMS3093H03;NSC-25412;SMR001548507

Suppliers and Price of 1-(3-Nitrophenyl)-1h-tetrazol-5-amine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 1-(3-Nitrophenyl)-1h-tetrazol-5-amine

Chemical Property:

Vapor Pressure:1.23E-08mmHg at 25°C
Boiling Point:459.8°C at 760 mmHg
Flash Point:231.9°C
Density:1.78g/cm³
XLogP3:0
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:1
Exact Mass:206.05522346
Heavy Atom Count:15
Complexity:244

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC(=C1)[N+](=O)[O-])N2C(=NN=N2)N

Technology Process of 1-(3-Nitrophenyl)-1h-tetrazol-5-amine

There total 8 articles about 1-(3-Nitrophenyl)-1h-tetrazol-5-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 709-72-8
3-nitrophenylthiourea

: 5467-77-6
1-(3-nitrophenyl)-1H-tetrazol-5-ylamine

: 152813-56-4
(3-nitro-phenyl)-(1H-tetrazol-5-yl)-amine

Guidance literature:: With sodium azide; ammonium cerium (IV) nitrate; triethylamine; In N,N-dimethyl-formamide; at 100 ℃; Overall yield = 93 percent; regioselective reaction; Green chemistry;
DOI:10.1016/j.jics.2021.100103

Reference yield:

: 5467-77-6
1-(3-nitrophenyl)-1H-tetrazol-5-ylamine

Guidance literature:: With hydrogenchloride; sodium nitrite; und anschliessend mit Na₂CO₃;
DOI:10.1021/ja01630a024 DOI:10.1021/jo50013a002

Reference yield:

: 3529-82-6
3-nitrophenyl isothiocyanate

: 5467-77-6
1-(3-nitrophenyl)-1H-tetrazol-5-ylamine

Guidance literature:: Multi-step reaction with 2 steps

1: ammonia / water / 0.33 h / 20 °C / Cooling with ice

2: sodium azide; iodine; triethylamine / N,N-dimethyl-formamide / 2.6 h / 20 °C

With sodium azide; ammonia; iodine; triethylamine; In water; N,N-dimethyl-formamide;
DOI:10.1039/c0ob01007c