Re₂Cl₆(P(C₂H₅)(C₆H₅)2)2

Base Information

Chemical Name:Re₂Cl₆(P(C₂H₅)(C₆H₅)2)2
CAS No.:55661-10-4
Molecular Formula:C₂₈H₃₀Cl₆P₂Re₂
Molecular Weight:1013.63
Hs Code.:

Re<sub>2</sub>Cl<sub>6</sub>(P(C<sub>2</sub>H<sub>5</sub>)(C<sub>6</sub>H<sub>5</sub>)2)2

Synonyms:Re₂Cl₆(P(C₂H₅)(C₆H₅)2)2

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Chemical Property of Re₂Cl₆(P(C₂H₅)(C₆H₅)2)2

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Technology Process of Re₂Cl₆(P(C₂H₅)(C₆H₅)2)2

There total 1 articles about Re₂Cl₆(P(C₂H₅)(C₆H₅)2)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 14023-10-0
tetra-n-butylammonium octachlorodirhenate(III)

: 607-01-2
ethyl-diphenyl-phosphane

: 55661-10-4
Re₂Cl₆(P(C₂H₅)(C₆H₅)2)2

Guidance literature:: With HCl; In methanol; Re-complex in MeOH, HCl and PEtPh2 were stirred under N2 for 0.5 h at room temp.;; filtered off, washed with MeOH; dried in vac.;;

Reference yield: 93.0%

: 1277-43-6,78206-33-4
cobaltocene

: 55661-10-4
Re₂Cl₆(P(C₂H₅)(C₆H₅)2)2

: 93806-27-0
(C₅H₅)2Co⁽¹⁺⁾*Re₂Cl₆(P(C₂H₅)(C₆H₅)2)2^(1-)=(C₅H₅)2CoRe₂Cl₆(P(C₂H₅)(C₆H₅)2)2

Guidance literature:: In acetone; Re-complex and cobaltocene were stirred for 0.5 h at room temp. under N2 in acetone, soln. was chilled to 0°C;; collected, washed with acetone, dried in vac.; elem. anal.;;

Reference yield: 70.0%

: 17084-13-8
potassium hexafluorophosphate

: 55661-10-4
Re₂Cl₆(P(C₂H₅)(C₆H₅)2)2

: 119072-55-8,7188-38-7
tert-butylisonitrile

: 82544-36-3
[Re(tert-butyl isocyanide)4(PEtPh₂)Cl₂] hexafluorophosphate

Guidance literature:: In methanol; acetone; under N2, tert-butyl isocyanide syringed into soln. of Re complex in methanol, stirred and warmed gently for 1 h, taken to dryness, KPF6 dissolved in acetone added, soln. stirred for 10 min; added slowly 1:1 diethyl ether-hexane mixt., recrystd. from CH2Cl2-diethyl ether mixt., elem. anal.;