Tetrabutylammonium octachlorodirhenate(III)

Base Information

Chemical Name:Tetrabutylammonium octachlorodirhenate(III)
CAS No.:14023-10-0
Molecular Formula:C32H72Cl8N2Re2
Molecular Weight:1140.98
Hs Code.:
European Community (EC) Number:623-268-6
DSSTox Substance ID:DTXSID20583461
Mol file:14023-10-0.mol

Synonyms:Tetrabutylammonium octachlorodirhenate(III);14023-10-0;tetrabutylazanium;tetrachlororhenium(1-);DTXSID20583461;N,N,N-Tributylbutan-1-aminium tetrachlororhenate(1-) (1/1)

Suppliers and Price of Tetrabutylammonium octachlorodirhenate(III)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
Tetrabutylammonium octachlorodirhenate(III) 98%
1g
$ 144.00

American Custom Chemicals Corporation
TETRABUTYLAMMONIUM OCTACHLORODIRHENATE(III) 95.00%
1G
$ 730.68

Total 11 raw suppliers

Chemical Property of Tetrabutylammonium octachlorodirhenate(III)

Chemical Property:

PSA：0.00000
LogP:4.04860
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:24
Exact Mass:1140.22318
Heavy Atom Count:44
Complexity:135

Purity/Quality:

99% ^*data from raw suppliers

Tetrabutylammonium octachlorodirhenate(III) 98% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:Xi
Statements: 36/37/38
Safety Statements: 26-37/39

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Canonical SMILES:CCCC[N+](CCCC)(CCCC)CCCC.CCCC[N+](CCCC)(CCCC)CCCC.Cl[Re-](Cl)(Cl)Cl.Cl[Re-](Cl)(Cl)Cl

Technology Process of Tetrabutylammonium octachlorodirhenate(III)

There total 13 articles about Tetrabutylammonium octachlorodirhenate(III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 7647-01-0,15364-23-5
hydrogenchloride

: 1643-19-2
tetrabutylammomium bromide

: 98-88-4
benzoyl chloride

: tetrabutylammonium perrhenate

: 14023-10-0
tetra-n-butylammonium octachlorodirhenate(III)

Guidance literature:: benzoyl chloride; tetrabutylammonium perrhenate; at 210 ℃; for 5h; Inert atmosphere;

hydrogenchloride; tetrabutylammomium bromide; In ethanol; at 210 ℃; for 1.5h; Inert atmosphere;
DOI:10.1039/c6nj02393b

Reference yield: 95.0%

: tetrabutylammonium hexachlororhenate(IV)

: 14023-10-0
tetra-n-butylammonium octachlorodirhenate(III)

Guidance literature:: With hydrogenchloride; tetrabutylammomium bromide; benzoyl chloride; In ethanol; complex was refluxed in benzoyl chloride for 1.5 h, HCl saturated soln.of Bu4NBr in ethanol was added to a cooled mixture, refluxed for 1 h, under positive pressure of N2; concn., filtration, washing with ethanol, diethyl ether, drying in vac.;

Reference yield: 95.0%

: 98-88-4
benzoyl chloride

: tetrabutylammonium perrhenate

: 14023-10-0
tetra-n-butylammonium octachlorodirhenate(III)

Guidance literature:: With hydrogenchloride; tetrabutylammomium bromide; In ethanol; n-Bu4NReO4 was refluxed in benzoyl chloride for 1.5 h, HCl saturated soln. of Bu4NBr in ethanol was added to a cooled mixture, refluxed for 1 h, under positive pressure of N2; concn., filtration, washing a ppt. with ethanol and diethyl ether, ddying in vac.; elem. anal.;