N-Z-γ-tert-butylglutamyl-histidyl-D-sarcolysyl-N-^ω-nitroarginyl-tryptophyl-glycine

Base Information

• Chemical Name: N-Z-γ-tert-butylglutamyl-histidyl-D-sarcolysyl-N-^ω-nitroarginyl-tryptophyl-glycine
• CAS No.: 85642-55-3
• Molecular Formula: C₅₅H₇₀Cl₂N₁₄O₁₃
• Molecular Weight: 1206.15

Synonyms:N-Z-γ-tert-butylglutamyl-histidyl-D-sarcolysyl-N-^ω-nitroarginyl-tryptophyl-glycine

Chemical Property of N-Z-γ-tert-butylglutamyl-histidyl-D-sarcolysyl-N-^ω-nitroarginyl-tryptophyl-glycine

Chemical Property:

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Technology Process of N-Z-γ-tert-butylglutamyl-histidyl-D-sarcolysyl-N-^ω-nitroarginyl-tryptophyl-glycine

There total 7 articles about N-Z-γ-tert-butylglutamyl-histidyl-D-sarcolysyl-N-^ω-nitroarginyl-tryptophyl-glycine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

N-Z-γ-tert-butylglutamyl-histidyl-D-sarcolysyl-Nω-nitroarginyl-tryptophyl-glycine methyl ester (85642-53-1) → N-Z-γ-tert-butylglutamyl-histidyl-D-sarcolysyl-N-ω-nitroarginyl-tryptophyl-glycine (85642-55-3)

Guidance literature:

With sodium hydroxide; In water; acetone; for 2h; Ambient temperature;

Reference yield:

N-formylsarcolysine (26367-45-3) → N-Z-γ-tert-butylglutamyl-histidyl-D-sarcolysyl-N-ω-nitroarginyl-tryptophyl-glycine (85642-55-3)

Guidance literature:

Multi-step reaction with 4 steps

1: 73 percent / (C₂H₅)3N, dicyclohexylcarbodiimide / dimethylformamide / 19 h / Ambient temperature

2: 91 percent / HCl / methanol / 8 h / Ambient temperature

3: 69 percent / (C₂H₅)3N / ethyl acetate; dimethylformamide / 48 h / 4 °C

4: 78 percent / NaOH / H₂O; acetone / 2 h / Ambient temperature

With hydrogenchloride; sodium hydroxide; triethylamine; dicyclohexyl-carbodiimide; In methanol; water; ethyl acetate; N,N-dimethyl-formamide; acetone;

Reference yield:

(S)-4-[(S)-1-Azidocarbonyl-2-(1H-imidazol-4-yl)-ethylcarbamoyl]-4-benzyloxycarbonylamino-butyric acid tert-butyl ester (51221-20-6) → N-Z-γ-tert-butylglutamyl-histidyl-D-sarcolysyl-N-ω-nitroarginyl-tryptophyl-glycine (85642-55-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 69 percent / (C₂H₅)3N / ethyl acetate; dimethylformamide / 48 h / 4 °C

2: 78 percent / NaOH / H₂O; acetone / 2 h / Ambient temperature

With sodium hydroxide; triethylamine; In water; ethyl acetate; N,N-dimethyl-formamide; acetone;

upstream raw materials:

N-Z-γ-tert-butylglutamyl-histidyl-D-sarcolysyl-N^ω-nitroarginyl-tryptophyl-glycine methyl ester

N-formylsarcolysine

(S)-4-[(S)-1-Azidocarbonyl-2-(1H-imidazol-4-yl)-ethylcarbamoyl]-4-benzyloxycarbonylamino-butyric acid tert-butyl ester

N-formyl-D-sarcolysyl-N^ω-nitroarginyl-tryptophyl-glycine methyl ester

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