3-phenoxyphenoxyethyl thiocyanate

Base Information

Chemical Name:3-phenoxyphenoxyethyl thiocyanate
CAS No.:1487429-08-2
Molecular Formula:C₁₅H₁₃NO₂S
Molecular Weight:271.34
Hs Code.:

Synonyms:3-phenoxyphenoxyethyl thiocyanate

Suppliers and Price of 3-phenoxyphenoxyethyl thiocyanate

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Chemical Property of 3-phenoxyphenoxyethyl thiocyanate

Chemical Property:

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Technology Process of 3-phenoxyphenoxyethyl thiocyanate

There total 5 articles about 3-phenoxyphenoxyethyl thiocyanate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1487429-06-0
3-phenoxyphenoxyethyl 4-toluenesulfonate

: 333-20-0
potassium thioacyanate

: 1487429-08-2
3-phenoxyphenoxyethyl thiocyanate

Guidance literature:: In N,N-dimethyl-formamide; at 100 ℃; for 6h;
DOI:10.1016/j.ejmech.2013.09.009

Reference yield:

: 1487429-02-6
2-(3-iodophenoxy)ethyl tetrahydro-2H-pyran-2-yl ether

: 1487429-08-2
3-phenoxyphenoxyethyl thiocyanate

Guidance literature:: Multi-step reaction with 4 steps

1.1: copper(l) iodide; 2-Picolinic acid; potassium phosphate / Inert atmosphere

1.2: 24 h / 80 °C

2.1: pyridinium p-toluenesulfonate / methanol / 14 h / 20 °C

3.1: pyridine / 3 h / 0 °C

4.1: N,N-dimethyl-formamide / 6 h / 100 °C

With pyridine; 2-Picolinic acid; potassium phosphate; copper(l) iodide; pyridinium p-toluenesulfonate; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2013.09.009

Reference yield:

: 626-02-8
3-Iodophenol

: 1487429-08-2
3-phenoxyphenoxyethyl thiocyanate

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium hydroxide / dimethyl sulfoxide / 0.5 h / 20 °C

1.2: 16 h / 20 °C

2.1: copper(l) iodide; 2-Picolinic acid; potassium phosphate / Inert atmosphere

2.2: 24 h / 80 °C

3.1: pyridinium p-toluenesulfonate / methanol / 14 h / 20 °C

4.1: pyridine / 3 h / 0 °C

5.1: N,N-dimethyl-formamide / 6 h / 100 °C

With pyridine; 2-Picolinic acid; potassium phosphate; copper(l) iodide; pyridinium p-toluenesulfonate; potassium hydroxide; In methanol; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2013.09.009