C₂₂H₂₇N₅O₃

Base Information

Chemical Name:C₂₂H₂₇N₅O₃
CAS No.:1558037-36-7
Molecular Formula:C₂₂H₂₇N₅O₃
Molecular Weight:409.488
Hs Code.:

C<sub>22</sub>H<sub>27</sub>N<sub>5</sub>O<sub>3</sub>

Synonyms:C₂₂H₂₇N₅O₃

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Chemical Property of C₂₂H₂₇N₅O₃

Chemical Property:

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Technology Process of C₂₂H₂₇N₅O₃

There total 5 articles about C₂₂H₂₇N₅O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 1558038-65-5
C₁₉H₂₅N₅O₂

: 79-10-7
acrylic acid

: 1558037-36-7
C₂₂H₂₇N₅O₃

Guidance literature:: With N-ethyl-N,N-diisopropylamine; HATU; In N,N-dimethyl-formamide;

Reference yield:

: 1147557-97-8
6-hydroxy-2-aza-spiro[3.3]heptane-2-carboxylic acid tert-butyl ester

: 1558037-36-7
C₂₂H₂₇N₅O₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine; dmap / dichloromethane / 24 h

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 18 h / 70 °C

3.1: hydrido(dimethylphosphinous acid κP)[hydrogen bis(dimethylphosphinito-κP)]platinum(II) / water; ethanol / 80 °C

3.2: 20 °C

4.1: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide

With dmap; hydrido(dimethylphosphinous acid κP)[hydrogen bis(dimethylphosphinito-κP)]platinum(II); sodium hydride; triethylamine; N-ethyl-N,N-diisopropylamine; HATU; In ethanol; dichloromethane; water; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 1558037-97-0
6-(toluenesulfonyloxy)-2-azaspiro[3.3]heptane-2-carboxylic acid tert-butyl ester

: 1558037-36-7
C₂₂H₂₇N₅O₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 18 h / 70 °C

2.1: hydrido(dimethylphosphinous acid κP)[hydrogen bis(dimethylphosphinito-κP)]platinum(II) / water; ethanol / 80 °C

2.2: 20 °C

3.1: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide

With hydrido(dimethylphosphinous acid κP)[hydrogen bis(dimethylphosphinito-κP)]platinum(II); sodium hydride; N-ethyl-N,N-diisopropylamine; HATU; In ethanol; water; N,N-dimethyl-formamide; mineral oil;